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Document / 9 pages

GCMS calibration table review, Jan-Feb 2002

Machine-extracted title · confidence 100%

Laboratory document detailing GC/MS calibration data for various compounds and method parameters reviewed on January 9, 2002.

NYC-WTC_000016383–000016391

Folder label: “GCMS X 12/24/01 A 1/9/02 2/15/02

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Scanned page image, NYC-WTC_000016389
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\JAN0 802\31344.D Vial: 11 Acq On 9 Jan 2002 11:33 pm Operator: 209 GALOS Sample gems scan 12/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

14.17 0.27 ug/1 98041 Naphthalene-d8 15.12

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopentasi xane, decamethyl- 370 C10H3005Si5 000541-02-6 64 2 Benzoic acid , 2,5-bis(trimethylsilo 370 C16H30O4Si3 003618-20-0 43 3 Benzeneethanamine, N-[ (pentafluorop 475 C21H26F5NO2Si2 055429-85-1 37 4 Benzene hanamine, N-[(pentafluorop 563 C24H34F5NO3Si3 055429-13-5 37 Abundance 7 Scan 994 (14.166 min): 31344.D (-) m/z 73.00 100.00% 73

5000 267 355 45 108 133 154 177193 223 251 1 13.80 14.00 .14.20 14.40 I TOUTumumuumm ‘11 “ —nmmpa ■ i ■ ‘ ' i ‘"339 1" ‘I m/z 267.00 33.44% miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73 355 - 267 5000 13.80 14.00 14.20 14.40 m/z 355.05 21.54% 191207 251 323339 | m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #7378: Berzolc acki 2 S-bistki 73 355 _________ /__________ ■ । ‘ । ‘ । ■ i • ■ ■ • । ■ 13.80 14.00 14.20 14.40 5000 m/z 74.00 9.12% 45 147 179 207223 267282297 370 114mt44rT!0—0mpd1mn—ma101010umnmuu—ImroT miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #74573: Benzeneethanamine, N-[(pentafluorophenyl)methylene] TT T T 18 73 13.80 14.00 14.20 1440 m/z 356.0 7.68% 5000 267

miz-> m 4............ 151 , 179194299 .... 250 . ...... 44

40 60 80 100 120 140 160 180 ‘260’ ‘220 240 ‘260' 280 300 '320 340 360 '' 1 I • 1 1 1 I ‘ ‘ 13.80 14.00 14.20 14.40 -n-pr-n-r-p-

31344.D GCMS0103 .M Wed Feb 06 11:24:50 2002 Page 2 NYC-WTC_000016389

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NYC-WTC_000016389Source: NYC Law Department, mirrored locally

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