Laboratory document detailing GC/MS calibration data for various compounds and method parameters reviewed on January 9, 2002.
NYC-WTC_000016383–000016391Folder label: “GCMS X 12/24/01 A 1/9/02 2/15/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\l\DATA\JAN0802\31344.D Vial: 11 Acq On 9 Jan 2002 11:33 pm Operator: 209 GALOS Sample gems scan 12/24 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Phenanthrene-diO Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T.
24.95 0.23 ug/1 85717 Phenanthrene-dl0 24.81
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phenanthrene -d10 188 C14D10 001517-22-2 56 2 2-Quinolinecarboxaldehyde, 8-hydrox 188 C10H8N2O2 005603-22-5 47 3 Naphthalene, 2,6-dimethoxy- 188 C12H1202 005486-55-5 47 4 4-Methyl/2-(4-fluorophenyl)pyrimidi 188 C11H9FN2 076128-67-1 47 Abundance Scan 2169 (24.953 min): 31344.D (-) m/z 188.10 100.00% 188
5000
24.60 24.80 25.00 25.20 ' TT m/z 80.00 19.79% miz-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 168
5000 24.60 24.80 25.00 ‘25'20 ' ' ’ ‘ m/z 94.00 15.59%
m/z-> RR 00 80! 94; ,I,U.Iii..!...,| .1,|..,.|....|Il..| , m mPP 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 160
Abundance #69185: 2-umolinecarboxaldebyde 8-ydroxy, oio 188
24.60 24.80 25.00 25.20 ' ' ‘ 5000 m/z 189.10 13.81% 143 64 89 116 130 158 170 TIPIDmWupggoTogunfngoontuado1a101(2mamn9mp309299990922—2—22977T miz-> Abundance 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 #19908: Naphthalene, 2,6-dimethoxy- ' i 1 ' y......... i > ; T । » FT j 11 * 1-| ’ 188 24.60 24.80 25.00 25.20 173 m/z 160.05 11.66% 145 5000 102 114 130 76 94 I m/z-> TIWWTLTTTTTTTTTTTTTTTTTT 111 ■1 ‘11 ■ ■' outt 1157. plimir 1233 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ’*1*11 24.60 24.80 25.00 25.20
31344.D GCMS0103.M Wed Feb 06 11:24:54 2002 Page 3
NYC- WTC_000016390
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