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GCMS sample analysis report for AD29927, Jan 2002

Machine-extracted title · confidence 100%

Laboratory analysis report for environmental sample AD29927 showing GCMS results and surrogate compound recovery rates.

NYC-WTC_000037437–000037447

Folder label: “GCMS X 12/11/01 A 12/16/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\DEC1401\29791A.D Vial: 47 Acq On : 16 Dec 2001 11:37 am Operator: 209 GALOS Sample : gems scan 12/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 3 Phenanthrene-diO Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

25.11 0.37 ug/1 122984 Phenanthrene-dl0 24.97

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene- 16 188 C14D10 001517-22-2 45 2 4-Methyl-2- (3 dI uorophenyl) pyrimidi 188 C11H9FN2 076128-66-0 43 3 Anthracene-d10- 188 C14D10 001719-06-8 25 4 3H-Naphthi 1,8-bc]thiophen-3-one, 4 188 C11H8OS 010245-79-1 23 Abundance Scan 2186 (25.115 min): 29791A.D (-) m/z 188.10 100.00% 188

5000 94 80

mlz—> 42 50 64 —HT m 180 — 132 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 146 156 24.80 25.00 25.20 25.40 m/z 94.00 26.68% Abundance #19958: Phenanthrene-d10 188

5000 - 24.80 25.00 25.20 25.40 rn/z 92.00 15.73% rr 80 94 1 60 66 | H.... ................... #....... ll... m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19859:4-Methyl-2-(3-fluorophenyl)pyrimidine 188 — —- 24.80 25.00 25.20 25.40 5000- 121 m/z 80.00 14.10%

67 173 94 75 146 161 I m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10- 188 24.80 25.00 25.20 25.40 m/z 184.10 12.43% 5000-

66 80 1IWWPIWNTLPNPTTTI 94 160 — m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 24.80 25.00 25.20 25.40

29791A.D GCMS1126.M Wed Jan 30 11:49:32 2002 Page 3

NYC-WTC_000037446

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NYC-WTC_000037446Source: NYC Law Department, mirrored locally

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