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GCMS sample analysis report with surrogate recovery, Jan 2002

Machine-extracted title · confidence 100%

Laboratory analysis report for environmental sample AD29781 showing GCMS results and surrogate compound recovery rates.

NYC-WTC_000037384–000037396

Folder label: “GCMS X 12/11/01 A 12/16/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC14O1\29926 .D Vial: 45 Acq On 16 Dec 2001 9:40 am Operator: 209 GALOS Sample gems scan 12/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Phenanthrene-diO Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

25.12 0.31 ug/1 101366 Phenanthrene-dl0 24.97

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthr he-d10// 4 188 C14D10 001517-22-2 53 2 Anthracene -diO- / 7 188 C14D10 001719-06-8 50 3 2-Quinolinecarboxaldehyde, -hydrox 188 C10H8N2O2 005603-22-5 38 4 Benzene, 1-(1-cyclohexen-l-yl)-4-me 188 C13H160 020758-60-5 28 Abundance 7 Scan 2186 (25.115 min): 29926.0 (-) m/z 183.10 100.00% 188

5000- 94 / 80 1 ' i '

- ■"I 47 66 10 132 .................. 146 TITT 109

40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 156 1— 24.80 25.00 25.20 25.40 m/z 94.00 27.67% Abundance #19958: Phenanthrene-d10 188

.......... / t.......................... 5000 24.80 25.00 25.20 25.40 m/z 79.95 19.87% RR 80 94 160

m/z—> 40 50 60 70 6 ,6 4ll....... .. —ill. 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d IQ- 188 J V 24.80 25.00 25.20 25.40 5000- m/z 189.00 16.60%

— 80 94 160 . li 66 । ! II ■ i ■' ■' i'1'' i'1 ■' i ■'' ■ I' i ■ ‘1' 11' ■' i " •' i ■11 ■ i'''' i ■1 ■ ■ i' ■' ■ i ■ ■ ■' i TTT TTT m/z--> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #69165: 2-Quinolinecarboxaldehyde, 8-hydroxy-, oxime / 'l1 188 24.80 25.00 25.20 25.40 m/ Z 15 . 00 11.85% 5000 143 64 89 116 130 |, 158 170 ■ r ■ ■' i' mmm - । < > I I— । THTPTTTTT T’T m/z-> 40 50 60 70 80 90 100 110 20 130 140 150 160 170 180 190 24.80 25.00 25.20 25.40

29926.D GCMS1126.M Wed Jan 30 11:50:30 2002 Page 3

NYC-WTC_000037395

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NYC-WTC_000037395Source: NYC Law Department, mirrored locally

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