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GCMS analysis results for sample AE10161, May 2002

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AE10161 conducted on May 10, 2002.

NYC-WTC_000044815–000044826

Folder label: “GCMS X 4/29/02 A 5/3/02”

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NYC 9/11 Public Portal Document

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Data File C: \HPCHEM\1\DATA\MAY0602\10161.D Vial: 9 Acq On 8 May 2002 1:40 am Operator: Sample GC/MS SCAN 4/29 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0507.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Phenanthrene-diO Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 25.71 0.43 ug/1 37383 Phenanthrene-dl0 25.58

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Phenanthrene'-d10/y 7 001517-22-2 93 188 C14D10 2 Anthracene7^10- / 001719-06-8 87 188 C14D10 3 2-Quinolinecarboxaldehyde, 8-hydrox 188 C10H8N2O2 005603-22-5 40 4 Pentacycho [8.4.0.0 (3,7) . 0 (4,14) .0 (6 188 C14H20 000000-00-0 36 Abundance / Scan 2256 (25.715 min): 10161.D (-) m/z 188.15 100.00% 188

5000

80 94 ..... H............... 1 I I I I I I I I I I I I I I I I I I "I I I I 160 i 25.40 25.60 25.80 26.00 44 54 66 ........... i j.... l —HTP i । i i i । । । > । ■ । । । n |’’’II । > । t । । । । । । । । । । । । । n pi । । i । । । m/ z 94.10 18.26% m/z—> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 188

"I I I I I A •I — I I I I I I [ — I I r 5000 25.40 25.60 25.80 26.00 m/ z 18 9.10 17.44% 80 94 160

m/z-> 30 40 50 60 66 70 80 90 100 110 120 130 140 150 160 170 180 190 l. L Tn p I I । J I I । i । i i TT

Abundance #19957: Anthracene-d10- 188 .. H...... 25.40 25.60 25.80 26.00 5000 m/z 80.10 13.00% fl e। 80I 94J I । | । I । > | ! > ! ! | I । । । | > > I I [ > > < > | I I I I | I I I I | I I I t [ I I I I | I I I I | I 160 ..... hill... m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #69165: 2-Quinolinecarboxaldehyde, 8-hydroxy-, oxime 188 4 25.40 25.60 25.80 26.00 m/z 160.10 10.53%

5000

143 89 ill। Eg 170 64 116 130 > • । ■ ■ > ■ । • ■ ■ ■ । ■ I ■ ■ i ‘11' i ‘11111111111111111 ‘‘i r 1 r ' । I | I 178 I, I | I I I I | I I ! 'I | I I I I | I I | 1 I [ I I — — I 1 I I I I I I [ I—I—I—I—I" TIT m/z-> 30 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.40 25.60 25.80 26.00

10161.D GCMS0507.M Thu May 09 11:12:48 2002 Page 4

NYC-WTC_000044825

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NYC-WTC_000044825Source: NYC Law Department, mirrored locally

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