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GCMS unknowns analysis report for sample AD31249, Feb 2002

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Laboratory analysis report from the DEP identifying unknown compounds in environmental sample AD31249 using GCMS on February 11, 2002.

NYC-WTC_000016929–000016939

Folder label: “GCMS X 12/24/01 A 1/10/02

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NYC 9/11 Public Portal Document Library Search Compound Report o Data File : C:\HPCHEM\1\DATA\JAN0902\31249.D Vial: 15 Acq On : 11 Jan 2002 5:14 am Operator: 209 GALOS Sample : gems scan 12/24 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Peereerrrrrrrrrere: fertrsrrsrrrererrtr ti tttcrttctt ttt tite rt ttt t tri ty Peak Number 2 Naphthalene, 2,6-dimethoxy- Concentration Rank 3 R.T. EstCone Area Relative to ISTD R.T. 24.95 0.23 ug/l 56875 Phenanthrene-d10 24.81 Hit# of 5 Tentative ID MW MolForm cas# Qual 1 Naphthalene, 4, 6-dimethoxy- 188 C12H1202 005486-55-5 53 2 Naphthaleng/ 1, 7-dimgthoxy- 188 C12H1202 005309-18-2 53 3 Phenanthrghe-dlo 188 C14D10 001517-22-2 45 _4 Anthracerle-d10-_ __188 C14D10 __001719-06-8 43 Abundance Sean 2169 (24.953 min}: 31248.D (-) a m/z —o 100.00: ‘5000: | re oe 132 146 158 24.60 _24:80_25.00_ 25.20 _ m/z 94.00 15.36: miz>__ 4080. 60. 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance: #19908: Naphthalene, 2,6-dimethoxy- 1 173 5 145 | bt 402 | 24.60 _24.80 25.00 25.20 a m/z 184.10 12.55) mn ow | om wt | mmiz->__|" 4” 80607060 80.100 110 120190 140_ 100 100 170 180 180 | Abundance AT Fechtheene. 7 2-dimeinoy= 173 188 24.60 24.80 25.00 25.20 000 m/z 189.10 11.12 102 nS 145 si 63 75 | 130 158 L | miz> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 100 | ‘Abundance — “#19968: Phenanthrene-d10 — — ' 1 24.60 24.80 25.00 25.20 j | [m/z 15B.05 9.36! 5000. | . | o oF 160 i mz->__""49'"80" 60 70 80 90 100 110 120 130 140 150 160 170 100 190 | 24.60 24160 25.00 2520 | 31249.D GCMS0103.M Tue Feb 05 16:48:06 2002 Page 2 NYC-WTC_000016937

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NYC-WTC_000016937Source: NYC Law Department, mirrored locally

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