GCMS analysis results for sample AE02596, Mar 2002

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Laboratory report documenting GCMS analysis of sample AE02596 conducted on March 7, 2002, including surrogate recovery data.

NYC-WTC_000005271–000005280

Folder label: “GCMS X 2/5/02 A 3/1/02”

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NYC 9/11 Public Portal Document Library Search Compound Report

Data File C:\HPCHEM\l\DATA\MAR0102\2596.D Vial: 6 Acq On 1 Mar 2002 1:16 pm Operator: Sample gc/ms scan 2/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Naphthalene, 1,7-dimethoxy- Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

25.85 0.22 ug/1 26530 Phenanthrene-dl0 25.71 O Hit# of 5 Tentative ID ‘ MW MolForm CAS# Qual Q7 1 Naphthalene, 1,7-dimethoxy- g 188 C12H1202 005309-18-2 53 2 Naphthalene, 2,6-dimethoxy 188 C12H1202 005486-55-5 42 3 Naphthalene, 1,5-dimethoxy 188 C12H1202 010075-63-5 42 4 Phenanthrene-d10 t Scan 2267 (25.851 min): 2596.D (-) 188 C14D10 001517-22-2 38 Abundance m/z 188.10 100.00% 11’8

5000 ........................ .........................

m/z-> 40 44 . .............. 50 60 66

70 80 92 .... 11,,, । ■1 ■ i''1' । ■111 80 90 100 110 120 130 140 150 160 170 180 190 160 L 1_____ 25.60 25.80 26.00 26.20 _ ] > ■ > l | ■ > > > | ■ mFl । IIT —m/z 189.10 19.41% Abundance #19913: Naphthalene, 1,7-dimethoxy- 173 188

5000 25.60 25.80 26.00 26.20 115 145 102 m/z 91.95 11.16% 51 63 75 94 130 158 1IWIpugu*BmpnmpnnaTu, TTPTTTTTTITTTTITTTTWTTITTT)PWTT)TT m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance '188 173 145 25.60 25.80 26.00 26.20 5000 m/z 94.00 10.15% 102

76 94 114 1o0 157 TT i ■ ■ ■ ■ i ■1 r' i111 ■ i'1 ■11 ■1 ■ ■ r1 iiti 1111 r ■'111111111'1111 m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19912: Naphthalene, 1.5-dimethoxy- 188 25.60 25.80 26.00 26.20 173 m/z 65.95 9.32% 115 5000-

_ 102 143 .............................. ......................... - 51 63 76 94 । 127 I, 1 ,, *' I'1 *11''1' I ITTn 117 11 1111 n । 11, । 111 i1 1 ■ J । | 1’1 i ' “ ' l i ■11 1 i'1 ■11 '' m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.60 25.80 26.00 26.20 |

2596.D GCMS0208.M Mon Mar 04 11:40:22 2002 Page 2

NYC-WTC_000005279

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