GCMS analysis results for sample AE06413, April 23, 2002

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\APR1202\6413.D Vial: 8 Acq On : 15 Apr 2002 2:56 pm Operator: Sample : re-extract Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Phenanthrene-diO Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 25.75 0.20 ug/1 35530 Phenanthrene-dl0 25.61 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Phenanthrene-dl 188 C14D10 001517-22-2 72 2 Anthracene-dio/ 188 C14D10 001719-06-8 64 3 Naphthalene, 1,7-dimethoxy- 188 C12H12021 005309-18-2 59 4 Naphthalene,/2,6-dimethoxy- 188 C12H1202 005486-55-5 40 Abundance Scan 2256 (25.754 min): 6413. D (-) m/z 188.10 100.00% 188

5000 . 2) T . 49 AR 66 80 | 94 158 25.40 25.60 25.80 26.00 11[. (, I , l । , . I r [ i i I i [1 113 m/z 184.10 17.51% miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19958: Phenanthrene-d10 188

5000 25.40 25.60 25.80 26.00 ' m/z 189.05 15.15% 80 94 160 1■i1 । । 66■ i ■ ■ - - mfa-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19957: Anthracene-d10- 118 . 9 25.40 25.60 25.80 26.00 1 5000 m/z 93.95 13.95%

66 80 94 160 “I ■TMI i | | i rl . । ■ i i i I > 111::-"1122119331011110210711 - nz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance #19913: Naphthalene, 1,7-dimethoxy- 173 188 25.40 25.60 25.80 26.00.. m/z 80.00 12.01% 5000 102 115 145

51 63 75 94 130 158 । BIIuumnaBmammmtiat 11' 111 “ P 1 ■'I-1''■!" I 1 ■i‘।111' i1 “ ■ i •1 “ i “ 1‘" — m/z—> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.40 25.60 25.80 26.00 ‘ ' 1 '

6413.D GCMS0412.M Tue Apr 16 15:40:55 2002 Page 3

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