GCMS analysis results for sample AE06413, April 23, 2002

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Library Search Compound Report Data File : C:\HPCHEM\1\DATA\APR12O2\6413.D Vial: 8 Acq On : 15 Apr 2002 2:56 pm Operator: Sample : re-extract Inst : 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0412.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 14.83 1.44 ug/1 227835 Naphthalene-d8 15.87 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 2 3,4-Dihydroxybenzyl alcohol, tris (tr 356 C16H32O3Si3 068595-79-9 46 3 Benzoic acid 2,4-bis[(trimethylsil 370 C16H30O4Si3 010586-16-0 43 4 N- (Trifluoro cetyl)^,0,0',011-tetr 553 C22H42F3NO4Si4 000000-00-0 37 Abundance 7 Scan 1066 (14.830 min): 6413.D (-) m/z 73.00 100.00%! 73

5000 267 355 ■ ... .............................................................................................................................................................................................................................

45 1 108 133 154 177193 223 251 t 14.40 14.60 14.80 15.00 15.20 323339 [ i H “ * ‘ r ‘ M । n 11'| -i 111-| r j ri । it t ri’t rl i —Tg" i rf p' Fri |TTi I["* TPWTIETTTTT1 “1 ■ i m/z 267.00 46.41%I mfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 3Z) 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73

355 267 5000 14.40 14.60 14.80 15.00 15.20 m/z 355.05 46.18% , , 191207 251 |, 323339 ’1’’2191*11’0112009280’2001—000101ur PPm i * “ • i miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #49868:3,4-DihydroxybenzyI alcohol,tris(trimethylsily!)- 73 i 1 * ‘ * i • 1 1 t ■ ■ 14.40 14.60 14.80 15.00 15.20 5000 179 267 m/z 356.05 16.34 356 45 147 , 209 *1m00—237 , 7—ar 312 341 , ■ i “ • • । ।■ i “' ■ i “ “ i “ “ i1 21’16’1—0011-003001’’ mfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #73975: Benzoic add, 2,4-bis[(trimethylsilyl)oxy}-, trimet 73 14.40 14.60 14.80 15.00 15.20 m/z 267.90 12.15% 5000 355 45

133149 193 223 281 340 ’191—0TmamEmpamin phairpunnipani ■ p “ 111 ■ •11“1111 11 'l1' “ I ............ 2. n/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.40 14.60 14.80 15.00 15.20

6413.D GCMS0412.M Tue Apr 16 15:40:54 2002 Page 2

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