DEP GCMS data table, Jan-Feb 2002

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Multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.

NYC-WTC_000004706–000004768

Folder label: “GCMS X 1/31/02 A 2/28/02”

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB2 702\2148.D Vial: 26 Acq On : 28 Feb 2002 3:08 pm Operator: Sample : gc/ms scan 1/31 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Naphthalene, 1,7-dimethoxy Concent rat ion Rank 1

R.T. EstConc Area Relative to ISTD R.T.

25.86 0.24 ug/1 38312 Phenanthrene-dl0 25.72

Hit# of 5 Tentative ID / MW MolForm CAS# Qual

1 Naphthalene, 1,7-dimethoxy- 188 C12H1202 005309-18-2 53 2 Anthracene-dlO- 188 C14D10 001719-06-8 50 3 4-Methyl-2-(4-fluorophenyl)pyrimidi 188 C11H9FN2 076128-67-1 45 4 Phosphonic acid, (3-methyl-3-penten 188 C8H13O3P __ 022152-34-7 45 Abundance ' ” ................Scan 2267 925.857 min): 2148.D () m/z 188". 1 O' 100.00% 188

5000 ) 1 . 80 94 . 25.60 25.80 26.00 26.20 66 160 1 • । ■ ■ ■ ■ । ■1 ■i■11U■1■11 > । ■11 ■ • ■' ।1 ■111111 ■ i1 ■■ ■ i1■1'।>11■' ■11 •1'11111 11 ■' IL m/z 79.95 13.70% m/z-> ... 40.... 50.... 60__ 70.... 80.... 90... 100.. 110 120 130 140.. 150 160 170 180 190 Abundance #19913: Naphthalene, 1,7-dimethoxy- 173 188

5000 115 25.60 25.80 26.00 26.20 102 145 m/z 93.95 12.43% 51 63 75 94 TIummBummnmmmgn< * i *11 * i11111111111111J1111111111 *' — 130 i 158 miz-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 Abundance 188

25.60 25.80 26.00 26.20 5000 m/z 189.10 11.86%

66 80 94 160

m/z-> .. 40 50 60 70 80 90 100 1W 120 130 140 150 160 170 180 190 Abundance #1 9860:4-Methyl-2-(4-fluoropheny!)pyrimidine 4 . ........... 188 25.60 25.80 26.00 26.20 121 m/ z .90 11.81% 5000 173 67 94 146 57 ■ ■ ■ ■ i ■' • ■ i ■ ■ 1 I ■ i1 75 ■ ■ ■ i ■ ■ •' i ‘ I. 102 | 1 ■11111111111 P 1111'1' * i *1 H । ■ ■ ■ * । * ■ * ■ । * !‘T V m/z-> 40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 25.60 25.80 26.00 26.20

2148.D GCMS0308.M Tue Mar 19 12:38:28 2002 Page 1

NYC-WTC_000004746

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NYC-WTC_000004746Source: NYC Law Department, mirrored locally

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