GCMS calibration results for sample AE03075, March 2002

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Laboratory report showing GC/MS calibration data and surrogate recovery for sample AE03075 on March 22, 2002.

NYC-WTC_000011091–000011095

Folder label: “GCMS X 2/12/02 A 3/19/02”

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Quantitation Report (QT Reviewed)

Data File C: \HPCHEM\ 1 \DATA\MARO 102\3075.D Vial: 27 Acq On 2 Mar 2002 11:52 am Operator : Sample gc/ms scan 2/12 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 5 14:08 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Internal Standards R.T. Qlon Response Cone Units Dev(Min)

1) 1,4-Dichlorobenzene-d4 12.32 152 433350 20.00 ug/1 -0.04 10) Naphthalene-d8 15.96 136 1705057 20.00 ug/1 -0.04 17) Acenaphthene-diO 21.27 164 898766 20.00 ug/1 -0.05 29) Phenanthrene-diO 25.72 188 1317462 20.00 ug/1 -0.05 38) Chrysene-dl2 33.79 240 916847 20.00 ug/1 -0.06 44) Perylene-dl2 38.06 264 613072 20.00 ug/1 -0.07

System Monitoring Compounds 37) 2,4-DDD 30.80 235 61510 4.47 ug/mL 0.30 Spiked Amount 5.000 Recovery = 89.40%

Target Compounds Qvalue 2) N-nitroso-dimethyl amine 5.50 74 192 N.D. 3) bis(2-Chloroethyl)ether 11.56 93 1037 N.D. 4) 1,3-Dichlorobenzene 0.00 146 0 N.D. 5) 1,4-Dichlorobenzene 0.00 146 0 N.D. 6) 1,2-Dichlorobenzene 0.00 146 0 N.D. 7) 2,2'-oxybis(1-Chloropropan 0.00 45 0 N.D. 8) N-Nitroso-di-n-propylamine 0.00 70 0 N.D. 9) Hexachloroethane 0.00 117 0 N.D. 11) Nitrobenzene 0.00 77 0 N.D. 12) 1sophorone 0.00 82 0 N.D. 13) bis(2-Chloroethoxy)methane 0.00 93 0 N.D. 14) 1,2,4-Trichlorobenzene 0.00 180 0 N.D. 15) Naphthalene 16.02 128 231 N.D. 16) Hexachlorobutadiene 0.00 225 0 N.D. 18) Hexachlorocyclopentadiene 0.00 237 0 N.D. 19) 2-Chloronaphthalene 0.00 162 0 N.D. 20) Dimethylphthalate 20.63 163 1482 N.D. 21) 2,6-Dinitrotoluene 0.00 165 0 N.D. 2 2) Acenaphthylene 0.00 152 0 N.D. 2 3) Acenaphthene 0.00 153 0 N.D. 24) 2,4-Dinitrotoluene 0.00 165 0 N.D. 25) Diethylphthalate 22.74 149 2461 N.D. 26) 4-Chlorophenyl-phenylether 0.00 204 0 N.D. 27) Fluorene 22.88 166 305 N.D. 2 8) Azobenzen/ 1,2-Diphenylhyd 0.00 77 0 N.D.

(#) = qualifier out of range (m) = manual integration 3075.D GCMS0308.M Fri Mar 22 18:06:04 2002 Page 1

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GCMS calibration table for TCLP analysis, March 2002 · Box DEP Box 14

NYC-WTC_000011949

Technical record of GCMS calibration data for TCLP analysis using sample vial 14 from March 28, 2002.

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