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GCMS calibration results for sample AE03075, March 2002

Machine-extracted title · confidence 100%

Laboratory report showing GC/MS calibration data and surrogate recovery for sample AE03075 on March 22, 2002.

NYC-WTC_000011091–000011095

Folder label: “GCMS X 2/12/02 A 3/19/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\1\DATA\MAR0102\3075.D Vial: 27 Acq On 2 Mar 2002 11:52 am Operator: Sample gc/ms scan 2/12 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 5 14:08 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 3 3) Phenanthrene 25.78 178 2200 N.D. 3 4) Anthracene 25.91 178 901 N.D. 35) Di-n-butylphthalate 27.68 149 2458 N.D. 36) Fluoranthene 29.44 202 653 N.D. 39) Pyrene 30.09 202 732 N.D. 40) Butylbenzylphthalate 32.21 149 102 N.D. 41) Benzo(a)anthracene 33.79 228 2621 N.D. 42) Bis(2-ethylhexyl)phthalate 33.99 149 9262 N.D. 43) Chrysene 33.79 228 3063 N.D. 45) Di-n-Octylphthalate 0.00 149 0 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 48) Benzo(a)pyrene 38.06 252 2368 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 3075.D GCMS0308.M Fri Mar 22 18:06:08 2002 Page 2

NYC-WTC_000011092

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NYC-WTC_000011092Source: NYC Law Department, mirrored locally

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