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GCMS analysis results for sample AE02711, Mar 15, 2002

Machine-extracted title · confidence 90%

Laboratory report listing unknown compounds and surrogate recovery data for sample AE02711.

NYC-WTC_000005473–000005483

Folder label: “GCMS X 2/5/02 A 3/7/02

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NYC 9/11 Public Portal Document

Quantitation Report (QT Reviewed)

Data File C:\HPCHEM\l\DATA\MAR0702\2711.D Vial: 22 Acq On 8 Mar 2002 10:23 am Operator: Sample gc/ms scan 2/5 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: GOOFY.P Quant Time: Mar 13 14:31 2002 Quant Results File: GCMS0208.RES

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Last Update : Wed Feb 27 11:30:15 2002 Response via : Initial Calibration DataAcq Meth : GCMS0208

Compound R.T. Qlon Response Cone Unit Qvalue

30) N-Nitrosodiphenylamine 0.00 168 0 N.D. 31) 4-Bromophenyl-phenylether 0.00 248 0 N.D. 32) Hexachlorobenzene 0.00 284 0 N.D. 33) Phenanthrene 25.68 178 462 N.D. 34) Anthracene 25.68 178 462 N.D. 35) Di-n-butylphthalate 27.65 149 14620 N.D. 36) Fluoranthene 0.00 202 0 N.D. 3 9) Pyrene 0.00 202 0 N.D. 40) Butylbenzylphthalate 0.00 149 0 N.D. 41) Benzo(a)anthracene 33.76 228 2771 N.D. 42) Bis(2-ethylhexyl)phthalate 33.96 149 3363 N.D. 43) Chrysene 33.76 228 2771 N.D. 45) Di-n-Octylphthalate 36.16 149 3824 N.D. 46) Benzo(b)fluoranthene 0.00 252 0 N.D. 47) Benzo(k)fluoranthene 0.00 252 0 N.D. 48) Benzo(a)pyrene 38.03 252 3116 N.D. 49) Indeno(1,2,3-cd)pyrene 0.00 276 0 N.D. 50) Dibenz(a,h)anthracene 0.00 278 0 N.D. 51) Benzo(g,h,i)perylene 0.00 276 0 N.D.

(#) = qualifier out of range (m) = manual integration 2711.D GCMS0208.M Wed Mar 13 14:32:28 2002 Page 2

NYC-WTC_000005476

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NYC-WTC_000005476Source: NYC Law Department, mirrored locally

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