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GCMS unknowns analysis report for sample AD31249, Feb 2002

Machine-extracted title · confidence 95%

Laboratory analysis report from the DEP identifying unknown compounds in environmental sample AD31249 using GCMS on February 11, 2002.

NYC-WTC_000016929–000016939

Folder label: “GCMS X 12/24/01 A 1/10/02

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Scanned page image, NYC-WTC_000016938
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NYC 9/11 Public Portal Document ‘ Library Search Compound Report oan Data File : C:\HPCHEM\1\DATA\JAN0902\31249.D Vial: 15 Acq On : 11 Jan 2002) 5:14 am Operator: 209 GALOS Sample : gems scan 12/24 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L JESSIE ISIS SII ISIS IIIS SEI UI IOUS CISTI SHT SHI ISI IIE na Peak Number 3 Acetaldehyde Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 31.85 0.39 ug/l 65657 Chrysene-di2 32.84 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Acetaldehyde 44 C2H40 000075-07-0 3 2 Ethylene“oxide 44 C2H40 000075-21-8 2 3 Piperjdine, 1-nitro- 130 C5H10N202 007119-94-0 2 . ,fPropane ~---#4 C3H8___(000074-98-6 1 Abundances ‘Scan 2920 (31.847 min): 31245.0¢) [m/z 39.95 100.00 __31.60 31.80 32.00 32.20 A seep | Je 43.95 «39.47: maar __20__40 60 80 100120140” 160180" 200" Abundance ‘#36: Acetaldehyde: | 48 i 7 | | | ‘5000 | 31.60_31.80 32.00 32.20 | [m/z 35.90 0.90' mes __""90_ 40 000100. 160.180. bo. abo | | ‘Abundance PBr ER en wa 7 | 16 31.60 _31.80_32.00 32.20 5000 i [m/z 44.95 0.63 i] i | i mies 2040 69 80 100.120.140.100 180_200 indance 8! Piparidine, t-nliro- — 31.60_31.80 32.00 32.20 [m/z 38.05 0.47 5000. | 5s 84 7 | 130 | mee 2040" 60.8 "300" 120 140180. 180 200. (ae 74 32.00 _ 3220” 31249.D GCMS0103.M Tue Feb 05 16:48:11 2002 Page 3 NYC-WTC_000016938

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NYC-WTC_000016938Source: NYC Law Department, mirrored locally

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