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GCMS analysis report for sample AE01223, Feb 2002

Machine-extracted title · confidence 95%

Analytical results page for sample AE01223 processed on February 25, 2002, showing surrogate recovery data.

NYC-WTC_000009739–000009748

Folder label: “GCMS X 1/17/02 A 2/17/02

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Scanned page image, NYC-WTC_000009747
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB1502\1223.D Vial: 34 Acq On : 17 Feb 2002 1:22 am Operator: 209 GALOS Sample : gc/ms scan 1/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Acetaldehyde Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

44.69 0.43 ug/1 25197 Perylene-dl2 38.08

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Acetaldehyde ly 44 C2H40 000075-07-0 3 2 Ethylene/oxide 44 C2H40 000075-21-8 3 3 6-Methyl-l,2,3,4-tetrahydroquinoxal 208 C9H8N2S2 000000-00-0 2 4 Piperidine, 1-nitro- __________ 130 C5H10N2O2__ 007119-94-0 2 Abundance 6 Scan 4319 (44.691 min): 1223.D (-) m/z 39.95. 100.00% 40

5000 ■ ‘ i ■ ■ • ■ i ■ ■ ‘ i ‘ ■ i ' ■

44.40 44.60 44.80 45.00 73 207 253 ’ 141’11 1 I m/z 43.95 46.93% m/z-2............. 20 40 . 60__ 80 100 120 140 160 180 200 220 240 Abundance #36: Acetaldehyde 29 44

5000 44.40 44.60 44.80 45.00 m/ z 44.85 0.96% ........ .......■ 11 • > ■ > । miz- 20 40 60 80 100 120 140 160 180 200 220 240 Abundance 29 ' ' l ' ' ‘ ' i ' ' ‘ i ■ ‘ ‘ i ' ‘ 15 44 44.40 44.60 44.80 45.00 5000 m/z 35.90 0.95%

20 40 60 80__ 100 120 140 160 180 200 220 240 Abundance #24745: 6-Methyl-1,2,3,4-tetrahydroquinoxaline-2,3-dithione 40 44.40 44.60 44.80 45.00 m/z 252.85 0.56% 5000 148 51 63 77 89 0 104 208 164 II ■ ■ 1 1 1 ■ ' i ■ ' ■ ■ i ■ ■ ■ ■ i 1" IT ’i m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 44.40 44.60 44.80 45.00

1223.D GCMS0208.M Thu Feb 21 09:29:18 2002 Page 2

NYC-WTC_000009747

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NYC-WTC_000009747Source: NYC Law Department, mirrored locally

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