GCMS analysis results for sample AD31018, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\JAN0 802\31018.D Vial: 14 * Acq On 9 Jan 2002 2:01 am Operator: 209 GALOS Sample gems scan 12/20 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 17 Acetaldehyde Concentration Rank 16

R.T. EstConc Area Relative to ISTD R.T.

39.93 0.53 ug/1 67016 Perylene-dl2 36.90 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Acetaldehyde 44 C2H40 000075-07-0 3 2 Ethylene oxide 44 C2H40 000075-21-8 2 3 Propane 44 C3H8 000074-98-6 1 4 Carbamic acid, monoammonium salt 78 CH6N202 001111-78-0 1 Abundance ( Scan 3800 (39.930 min): 31018.D (-) m/ z 39.95 100.00%

5000

r 17 TT11 T | I J 1 | I I1! T | T IT II 39.60 39.80 40.00 40.20 77 91 133 191 207 281 111111 ■ ■ i1 • ■ • ।1 ■ ■ ■ i ■ ■ ■ ■ i ■ • ■ ■ i ■ ■ • ■ ।1 ■ ■ ■ i ■ ■ ■ ■ । l * ' 1 ‘ I ' 1 ‘ ‘ I TTTT m/z 43.95 39.94% m/z->_____ 20__ 40 60 80 100 120 140 160 180. 200 220 240. 260 280 Abundance...... ......... #36: Acetaldehyde 29 44

5000 Tmmpr I"T 111" T‘ " 39.60 39.80 40.00 40.20 m/z 35.90 0.84% ■ ■ ‘ • i ■ ■ ■ ■ i 1

m/z—? 20 40 60* 80 ' 100 120 140 160 180 ‘266' '226 ‘240’ 260 280 Abundance

15 29 44 IALAMAAAANAAM 39.60 39.80 40.00 40.20 5000 m/z 44.95 0.64%

mfe-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #62269: Propane 29 39.60 39.80 40.00 40.20 m/z 38.05 0.27% 5000 44 15 J ■ ■ i ' 1 I I T" ।j।। ।. 11. ।।।j >... । > 1।j.. ' l ‘ ‘ ‘ i ‘ ‘ m/z-> 20 40 60 80_ 100 120 140 180 180 200 220 240 260 280 39.60 39.80 40.00 40.20

31018.D GCMS0103.M Wed Jan 09 12:08:46 2002 Page 17

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