GCMS analysis results for sample AE05846, April 23, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File C: \HPCHEM\ 1 \DATA\APRO4 02\5846A.D Vial: 20 Acq On 4 Apr 2002 4:48 pm Operator: Sample gc/ms scan 3/12 Inst : GC/MS 209 Mise Multiplr: 2.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0408.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Acetaldehyde Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 43.44 1.49 ug/1 28517 Perylene-dl2 37.93 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Acetaldehyde 44 C2H40 000075-07-0 3 2 Carbon dioxide 44 CO2 000124-38-9 3 3 Ethyne// fluoro- 44 C2HF 002713-09-9 3 4 Ethylene AbundanceV oxide Scan 4183 (43.444 min): 5846A. D (-) 44 C2H40 000075-21-8 3 m/z 39.95 100.00% 43

5000

43.20 43.40 43.60 43.80 73 96 177191 209 282 m/z 43.90 56.44% miz->______ 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #36: Acetaldehyde 23 44 .

5000 43.20 43.40 43.60 43.80 m/z 44.95 1.29 Ji ■' i ■ ■ ■ ■ i ■ ■ ■ ■ i • ■ ■ ■ i ■ ■ ■ ■ i ■' ■ ■ i ■ ■ ■' i'' ■' i ■' ' i ।.... i •... t miz->______ 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #62263: Carbon dioxide 44

43.20 43.40 43.60 43.80 5000 m/z 95.80 0.62

16 - ■ ■ i ■ • ■ ■ i11 ■ ■ i • ■ • ■ ......................... ... ... 1.... । i ■ ■ ■ • i ■ ■ ■ ■ i ■ ■ • ■ i ’i’T rn/z—> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #35: Ethyne, fluoro- 44 43.20 43.40 43.60 43.80 m/z 49.00 0.54%

5000 31 13 I I mfz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 ' ‘ i ' • ■ ■ I ’ 1 1 1 1 1 43.20 43.40 43.60 43.80 ■ ' i ■ ■

5846A.D GCMS0408.M Tue Apr 16 08:16:53 2002 Page 3

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