GCMS analysis report for sample AE01221, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\FEB1502\1221.D Vial: 35 Acq On : 17 Feb 2002 2:20 am Operator: 209 GALOS Sample : gc/ms scan 1/17 Inst : GC/MS 209. Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Ethylene oxide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

42.42 0.45 ug/1 22638 Perylene-dl2 38.09

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Ethylene oxide 44 C2H40 000075-21-8 3 2 Acetaldehyde 44 C2H40 000075-07-0 3 3 6-Methyl-l,2,3,4-tetrahydroquinoxal 208 C9H8N2S2 000000-00-0 2 4 Piperidine, 1-nitro- _____ 130 C5H10N2O2 007119-94-0 2 Abundance d Scan 4071 (42.419 min): 1221.D(-) m/z 39. 95 100 .00% 43

5000

42.00 42.20 42.40 42.60 42.80 ■ ' I ■ ' ' 1 73 .................... 208 m/z 43.95 39.67% miz-> 20 40 60 80 100 120 140 160 180 200 . Abundance #37: Ethylene oxide 29

15 44 5000 42.00 42.20 42.40 42.60 42.80 m/z 35.90 1.15%

mz->_ —20P40 60 80 100 120 140 160 180 200 Abundance £284: Amtan 29 44 42.00 42.20 42.40 42.60 42.80 5000 m/z 44.95 0.84%

■ ■ i ' • ■ ■ i ■ ■ ■ ■ i ■ ‘ • ■ i ' ■ ■ • i ■ • ■ ■ i ‘ • ■ ■ > ‘ ‘ ■ i • • • ■ i ' • ■ ■ i ■■ m/z-> 20 40 60 80 100 120 140 160 180 200 Abundance #24745:6-Methyl-1,2,3,4-tetrahydrbquinoxaline-2,3-dithione 40 42.00 42.20 42.40 42.60 42.80 m/z 208.00 0.65% 5000 N N V V 148 63 77 90 208 51 89 104 164 J , , L , .I , 1 114 ■ i 1 1 1 ■ । ■ • ■ ■ । ‘ T — ‘II _ _________ 20 40 60 80 100 120 140 160 180 200 42.00 42.20 42.40 42.60 42.80

1221.D GCMS0208.M Thu Feb 21 09:28:27 2002 Page 2

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