GCMS sample results, AE00898, Feb 26, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB1102\898.D Vial: 32 Acq On : 12 Feb 2002 6:18 pm Operator: 209 GALOS Sample : GC/MS SCAN 1/14 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Ethylene oxide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

10.92 0.36 ug/1 27745 1,4-Dichlorobenzene-d4 12.35

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 Ethylene oxide 44 C2H4O 000075-21-8 3 2 Acetaldehyde 44 C2H4O 000075-07-0 3 3 Propane / 44 C3H8 000074-98-6 1 4 Carbamic acid, monoammonium salt 78 CH6N202 001111-78-0 1 Abundance • Scan 640 (10.922 min): 898.D (-) 4b m/z 39.95 ‘ 100.00%

5000 44

10.60 10.80 11.00 11.20 36 51 86 m/z 43.95 49.53% m/z->____ 5 10 15 20 25 30 35 40 45 50 55.. 60.. 65.. 70.. 75 80 85 90 Abundance #37: Ethylene oxide 29

15 44 5000 10.60 10.80 11.00 11.20 m/z 35.90 1.30% 12 26 : : mIWITDTITMPTPmLPmPITT m/z->____ 51015 20. 25 30 35 40 45.50 55 60 65 70 75 80 85_ 90 Abundance / 29 44 10.60 10.80 11.00 11.20 5000 m/z 44.95 0.85%

26 41 .. i •. •. i •... j. *.. j ।.... ।.... ।.... ।.... 11... 11... ।.... j.... । .... 11... 11 n.]n .. ।. 1111.. 111 m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #62269: Propane.... . ....... . ■ ■ i ■ ■ • ■ i ■ • 1 ■ i • ■ ■ ■ i ■ ■ 1 ■ । 29 10.60 10.80 11.00 11.20 m/z 38.05 0.67% 5000 39 44 15 26 —— TPHH m/z-> 5.10 15. 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 10.60 10.80 11.00 11.20

898.D GCMS0208.M Wed Feb 20 09:52:20 2002 Page 2

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