GCMS analysis summary, sample AD31375, Feb 2002

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN1502\31375.D Vial: 8 Acq On : 15 Jan 2002 5:47 pm Operator: 209 GALOS Sample : gc/ms scan 12/26 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Ethylene oxide Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

6.22 0.27 ug/1 62923 1,4-Dichlorobenzene-d4 11.50

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Ethylere oxide 44 C2H40 000075-21-8 3 2 Acetaldehyde 44 C2H40 000075-07-0 3 3 Propane 44 C3H8 000074-98-6 1 4 Carbamic acid, monoammonium salt 78 CH6N202 001111-78-0 1 Abundance Scan 128 (6.219 mln): 31375.D (-) m/ z 39.95 100.00% 4b

5000 44

1*0///— 36 5.80 6.00 6.20 6.40 6.60 47 51 59 TmTmmdmm*mm 85 —*mT • i • •• • i •»»•i••»•,•.•<।‘‘J' *11'' ’1 m/z 43.95 46.68% miz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #62267: Ethylene oxide 1.......... 1 29 44 15 5000 —— ——Rm r-n-n-r 5.80 6.00 6.20 6.40 6.60 m/z 35.90 1.87 26 ‘11 m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance * Acotaldehyde 29 AvwWW/W WAMw 44 5.80 6.00 6.20 6.40 6.60 5000 m/z 59.05 1.03

26 41 . | .... | .... | .... । ... I | M I ... | ... I | |, j | M . | .... | I 1 1 1 | 1 1 1 ITTTI/ IIIH m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance $ #62269: Propane AA/ TV YAA 5.80 6.00 6.20 6.40 6.60 m/z 44.95 0.84 5000 39 44

m/z-> 15 26 mH t 11. ।. ।. 11 +

5 | 11111111 > 1111111111 j' r i 1111111 11111111 11 1111111111

10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 TTTJ- 5.80 MMAA.MM 6.00 6.20 6.40 6.60

31375.D GCMS1126.M Mon Feb 04 15:05:55 2002 Page 1

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