GCMS analysis summary, sample AD31375, Feb 2002

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\JAN1502\31375.D Vial: 8 Acq On : 15 Jan 2002 5:47 pm Operator: 209 GALOS Sample : gc/ms scan 12/26 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 N-Ethylformamide Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

7.45 4.38 ug/1 1006750 1,4-Dichlorobenzene-d4 11.50

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 N-Ethylformamide 73 C3H7NO 000627-45-2 9 2 1,3-Dioxolane, 2-methyl- 88 C4H802 000497-26-7 9 3 1,3-Dioxclane, 2-pentadecyl- 284 C18H36O2 004360-57-0 9 4 Silane,_Itetramethyl- ___ _ 88 C4H12Si 000075-76-3 9 Abundance ” Scan 262 (7.449 min): 31375.D (-) " 73 . " . 00% 73

5000 43 1 i' ■ • ■ i • ■ r ■ i ■ •

11,1 57 11 87 103 7.20 7.40 7.60 7.80 0 m/z 43.0,5 33.59% miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #292: N-Ethylformamide 30 73

5000 44 58 7.20 7.40 7.60 7 80 m/z 41.0.0 11.99%

m/z-> 15.1 I ■ ■ i1 ■ 20 40 11.8 60_ 80 100 120 140 160 180 200 220 240 260 280 Abundance 6/002 ’ 3Dmoam jmciri 73 « r । I 11II] । i i i j 11i i" J11 1 7.20 7.40 7.60 7.80 5000 43 m/z 45.0,5 11.50% 58 27 • 87 i ' ' i' ■' ‘ i 1' ‘ ' i ' ‘ ‘ 1 1 1 ■ 1 1 i ■ ' ■ ■ i ■' ' 11 1 1 11 I ' 1 1 ' I i • ■ ■ • i i ' ' ‘ ' i ' ‘ ‘ ■ i ■ ' miz-> 20 40 60 80 100 120 140 160 180 200 220 240 280 280 Abundance #40191: 1,3-Dioxolane, 2-pentadecyl- —mmgT ITT i~i 11 73 7.20 7.40 7.60 7.80 m/z 71.0,0 7.10% 5000

43 57 86 99 1414/*,*41*4*/11+6*1***’I+AAAI4*+*1*1+-+1+***1**}I 256 283 l r , . /naf" 1 1 IITuPu | | ; miz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 7.20 7.40 7.60 7.80

31375.D GCMS1126.M Mon Feb 04 15:06:01 2002 Page 2

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