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GCMS unknowns analysis report for sample AD31250, Feb 2002

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Laboratory analysis report from the DEP identifying unknown compounds in environmental sample AD31250 using GCMS on February 11, 2002.

NYC-WTC_000016940–000016950

Folder label: “GCMS X 12/24/01 A 1/10/02

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NYC 9/11 Public Portal Document 4 Library Search Compound Report : Data File : C:\HPCHEM\1\DATA\JAN0902\31250.D Vial: 6 Acq on : 10 Jan 2002 8:25 pm Operator: 209 GALOS Sample : gems scan 12/24 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L GEIS IIS IIIS SE IIS IIE ISIS I IOI III TOI IOI TOSI I TOI ISI TIT A III Peak Number 1 Ethylene oxide . Concentration Rank 2 R.T, EstCone Area Relative to ISTD R.T. 5.28 0.28 ug/1 57115 1, 4-Dichlorobenzene-d4 11.53 Hit# of 5 Tentative ID MW MolForm cas# Qual _ 1 Ethylene oxide 44 C2H40 000075-21-8 3 2 Acetaldehyde 44 C2H40 000075-07-0 3 3 Propane 44 C3H8 000074-98-6 1 4 Caxbamic acid, monoammonium salt 78 CHEN202___001111-78-0 1 Abundance, ‘Scan 25 (6.277 min): 31250.D ¢) | m/z rr 100.00% | 540 5.20 5.30 5.40 5.50 5.60 5.70 oe eter the thee m/z 43.95 39.99) ma> ___5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 Abundance #62267: Ethylene oxide “ | Io. 15 | 5000: i | ’ : | 5.10 5.20 5.30 5.40 5.50 5.60 5.70 | m/z 35.90 3.198) \ | | mz-> __§ 10 15 20 25 30 35 40 45 50 55 60 65 a adel Abundance rea: Acta * 2 AS Seeger earn 5.10 5.20 5.30 5.40 5.50 5.60 5.70 5000: m/z 37.90 1.11 mian>__5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100. ‘Abundance #622655 Propane | 5.10 5.20 5.30 5.40 5.50 5.60 5.70 m/z 35.00 0.90 ‘5000 : 39 wa 15 | | mizzz__"§" 40.15 20 25 30 36 40 45 50 95 80.65 7075 BO. 65.80 5 100 | 6.10 6.20 6.50 540 550 560 5.70 | 31250.D GCMS0103.M Tue Feb 05 16:49:09 2002 Page 1 NYC-WTC_000016947

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NYC-WTC_000016947Source: NYC Law Department, mirrored locally

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