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GCMS unknowns analysis report for sample AD31250, Feb 2002

Machine-extracted title · confidence 95%

Laboratory analysis report from the DEP identifying unknown compounds in environmental sample AD31250 using GCMS on February 11, 2002.

NYC-WTC_000016940–000016950

Folder label: “GCMS X 12/24/01 A 1/10/02

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NYC 9/11 Public Portal Document . Library Search Compound Report é Data File : C:\HPCHEM\1\DATA\JAN0902\31250.D Vial: 6 Acq On : 10 Jan 2002 8:25 pm Operator: 209 GALOS Sample : gems scan 12/24 Inst : GC/MS 209 Misc : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L JESS SSIES SSIS III IOS ITI ISIS IIIS IIIS SOI ISIC IIIS OSI EI Peak Number 2 N-Ethylformamide Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.47 3.70 ug/l 759036 1, 4-Dichlorobenzene-d4 11.53 Hit# of 5 Tentative ID MW MolForm cas# Qual 1 N-Ethylformgnide 73 C3H7NO 000627-45-2 9 2 Silane, teyramethyl- 88 C4H12Si 000075-76-3 9 3 3-Pentano{, 3-methyl- 102 C6H140 000077-74-7 9 qi Butane,“2-methoxy-2-methyl- __102 C6H14O0____—=—_—=—-000994-05-8 9 ‘Rbundance ‘Scan 264 (7.474 min}: 312800 () m/z 73-00 100.008 | 5000. i « 7 7.20 740 7.60 _7.80 BLO aye Sli # ma m/z 43. 32.51% men> __10 20 30 49 6060 _70 80 90 100 ___1101| Abundance #292; N-Ethylformamide bi 73 . { 5000- orp 5 7.20 7.40 7.60 7.80 “ i m/z 45.05 11.66% wo | ; mz->__ 10 20 304006070880 100. 140 ‘Abundance HESS Silang, terariebs ; ae 7207.40 7.60 7.80 5000. m/z 41.00 11.40% 15 3t © ss ' 88. meo 10 80 Abundance #63573: 3-Pentanol, 3-methyl- 720740 7.60 7.60 [m/z 71.00 6.86: 5000- . 55 a ae a | ar | mie “Yo' a0 "30. do 90.60.70 ago 100 to. | 70 7h0” 780 780) 31250.D GCMs0103.M Tue Feb 05 16:49:13 2002 Page 2 NYC-WTC_000016948

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NYC-WTC_000016948Source: NYC Law Department, mirrored locally

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