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GCMS unknowns analysis report for sample AD31250, Feb 2002

Machine-extracted title · confidence 95%

Laboratory analysis report from the DEP identifying unknown compounds in environmental sample AD31250 using GCMS on February 11, 2002.

NYC-WTC_000016940–000016950

Folder label: “GCMS X 12/24/01 A 1/10/02

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Scanned page image, NYC-WTC_000016949
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NYC 9/11 Public Portal Document ., Library Search Compound Report : Data File : C:\HPCHEM\1\DATA\JAN0902\31250.D Vial: 6 Acq On =: 10 Jan 2002 8:25 pm Operator: 209 GALOS Sample : gems scan 12/24 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) . Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K. L Perererererrrrrrrrer tert tert frrererrrrrrrrrcrrrerrrccr rrr r err errr eres Peak Number 3 Anthracene-d10- Concentration Rank 3 R.T. EstCone Area Relative to ISTD R.T. 24.96 0.22 ug/l 54505 Phenanthrene-d10 24.80 ° Hit# of 5 Tentative ID MW MolForm cas# Qual 1 Anthracen a0 188 C14D10 001719-06-8 72 2 Phenanthyene-d10 188 C14D10 001517-22-2 72 3 5-Oxazpfecarboxamide, 2-phenyl- 188 C10HEN202 039819-42-6 37 4 Selenfde, ethyl 1-methyl-1-penten-3 188 C8H12Se 025128-48-7 33 ad ‘Scan 2169 (24.956 miny: 51250. () is | 0/2 188.10 100.00 | 5000: 94 36 44 52 880 132 158 24.60 24.80 25.00 25.20 = : m/z 94.00 25.23 imz->__30 40 80 607080 90.100 140 120 130 140 150.160 170 160 190, arcs Haast manawa | 1 a r Te 24160 24180 25.00.2520 m/z 189.10 ~ 20.50 so et a | giz» 36.40” 806070 80. 80 100 110 120 190 140 100.100 170 180 100 | | Abundance FIORE: Proce tnt. a | 188 | 24:60 24:80 _25.00_25.20 5000: m/z 184.10 17.50 oo 160 . SLL ee miz~>_ 30_40 50 60 70 80 90 100 110 120 130 140 150 160 170 180 190 ‘Abundance #19812; 5-Oxazolecarboxamide, 2-phenyl- errr | 116 14 168 |_24.60 ‘24180 25.00 (25.20 | Mm/z 65.95 10.04% 5000- | 89 | 63 105 I iH mz->__30_40 80 60 7080 90 100 110 120.130 140, 190.160 170 160 190 | 24.60 24.80 25.00 25.20 -| 31250.D GCMS0103.M Tue Feb 05 16:49:18 2002 Page 3 NYC-WTC_000016949

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NYC-WTC_000016949Source: NYC Law Department, mirrored locally

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