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GCMS unknowns analysis report for sample AD31275, Feb 2002

Machine-extracted title · confidence 95%

Laboratory analysis report from the DEP identifying unknown compounds in environmental sample AD31275 using GCMS on February 11, 2002.

NYC-WTC_000016992–000017003

Folder label: “GCMS X 12/24/01 A 1/10/02

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Scanned page image, NYC-WTC_000017002
OCR text

OCR status: ocr · source: ours

NYC 9/11 Public Portal Document a Library Search Compound Report Data File : C:\HPCHEM\1\DATA\JAN0902\31275.D Vial: 9 Acq On: 10 Jan 2002 11:22 pm Operator: 209 GALOS Sample : gems scan 12/24 Inst : GC/MS 209 Misc b Multiply: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0103.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L Pereeetet Srrntr er Sener tS tr rn A Steer rtrnrenr err rere r te Serer erat Tenants Peak Number 4 Phenanthrene-d10 Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 24.96 0.21 ug/l 57824 Phenanthrene-d10 24.80 Hit# of 5 Tentative ID MW MolForm cas# Qual ft Pronanchren aig? 1g8 c14p10 001517-22-2 90 2 Anthracene“d10- 188 C14D10 001719-06-8 86 3 - (4-Toly1) -3-methy1-pyrazol-5-one 188 C11H12N20 035496-19-6 47 4 Antipyrine _188_C11#12N20 000060-80-0 38 ‘Rbundanes = Sean B69 (24.060 min): ST27ED G) to | 72 7 100.008 “ woth eon 41 54 66 iL 18 492 48 198 24.60 24.80 25.00 25.20 ap thepettie aie - m/z 184.10 17.63 miz-> "40.5060 70 80 90 100 110 120 130 140 150 160 170 160 190 Abundance #19958: Phenanthrene-di0 zi | Wen 5000. |__24leo' 24190 25.00 25120 oo @ om 199 m/z 189.10 16.80 ‘e> "40" 506070 8-90 100 110 120 190. 140 190. 160170180150 | haa oer ee | 188 | 2460" ‘24'80. 25.00 25.20 5000. [m/z 4-09 14.19: : « 9 160 miz-> "40. 8060708090 100 110 120 190 140 150 160 170 160 100. ‘Abundance ‘#19863: -(4-Tolyl)-3-methyl-pyrazol-6-one 1 24.60 24.80 25.00 25.20 on m/z 79.95 13.00: 5000: ye : 119 i 8 | 146 miz->__""4080 6070, 80, 90 100 110 120 180. 140 160 100 170 100 190” | 2460 24160 25100 25.00 31275.D GCMS0103.M Tue Feb-05 16:50:42 2002 Page 4 NYC-WTC_000017002

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NYC-WTC_000017002Source: NYC Law Department, mirrored locally

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