GCMS sample results, AE00898, Feb 26, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB1102\898.D Vial: 32 Acq On : 12 Feb 2002 6:18 pm Operator: 209 GALOS Sample : GC/MS SCAN 1/14 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 2-Methyl-5-hexen-3-ol Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

8.23 0.28 ug/1 21371 1,4-Dichlorobenzene-d4 12.35

Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 2-Methyl-5-hexen-3-ol 114 C7H140 032815-70-6 9 2 1,3-Dioxolane 74 C3H602 000646-06-0 5 3 Formamide, N,N-dimethyl- 73 C3H7NO 000068-12-2 4 4 N-Ethyl formamide__ _____________ 73 C3H7NO __ _000627-45-2 4 Abundance / Scan 347 (8.232 min): 898.D (-) m/ z 73. 00 "T6 0.00% 73

5000 43 TTt • • 1 1 1 TTuBnTTeT 7.80 8.00 8.20 8.40 8.60 ** 51.55......... 11 “ “ । 86 ■ i’ “ ■ i ■■ ■ ■ । m/ z 43.05 40.01%

J miz-> 5 . 10 15 20 25.. 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #3017:2-Methyl-5-hexen-3-ol 73 55 43 5000 7.80 8.00 8.20 8.40 8.60 27 m/ z 40.95 15.56% 31 i •' ‘ ■ i “ " I ■" ■ i “ “ i' mH ■..... .................... miz—___ 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance *0206R ■ 3ifomvdlac 73

7.80 8.00 8.20 8.40 8.60 5000 44 m/z 45.05 14.59% 29 15 ; 19 Oanmuupuummmu—mummum]]]] | I . . . | l . . . |T-| I | , I 1 | | 1 | m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90__ Abundance #62527: Formamide, N,N-dimethyl- 44 73 7.80 8.00 8.20 8.40 8.60 m/z 38.95 10.25% 5000 30 15 TH ,3841 mmmmmmm 27 58 I “ ‘' I ‘ ‘' I ‘' 11' 11 • ■ ■ ■ । ■ ■ ■ ■ । ■ ■ ■ ■ i'4 ■ ■ । . ||... ... miz-?__ 5 10 15 20 25 30 35 . 40 45 50 55 60 65 70 75 80 85 90 7.80 8.00 8.20 8.40 8.60

898.D GCMS0208.M Wed Feb 20 09:52:15 2002 Page 1

NYC-WTC_000009453