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GCMS blank analysis report, Feb 2002

Machine-extracted title · confidence 95%

Blank sample analysis report confirming no contamination above method detection limits for target compounds analyzed on February 1, 2002.

NYC-WTC_000005159–000005166

Folder label: “GCMS X 2/4/02 A 2/8/02

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Scanned page image, NYC-WTC_000005165
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\FEB0802\LB.D Vial: 5 Acq On 8 Feb 2002 1:11 pm Operator: 209 GALOS Sample GC/MS SCAN 2/8 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 3,4-Dimethyl-5-hexen-3-ol Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.23 0.27 ug/1 25863 1,4-Dichlorobenzene-d4 12.35

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3,4-Dimethyl-5-hexen-3-ol 128 C8H16O 000000-00-0 9 2 N-Ethylformamide 73 C3H7NO 000627-45-2 4 3 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 4 4 2-Methyl-5-hexen-3-ol 114 C7H140 032815-70-6 4 Abundance Scan 347 (8.226 min): LB.D (-) | m/z 73.00 100.00% 73

5000 43 . ..

m/z-> 10 20 30 —lll 40 50 ■ 55... ,i - । ■ ■ ■ 60 87 TPTT j m/ z ' i 1 1 70 103 80 7.80 r----- 1 1 i 1 — 8.00 8.20 8.40 8.60 43.0.5 45.25% 90 100 110 | Abundance #5018: 3.4-D methyl-5-hexen-3-ol 73

5000 43 55 !- . h. 7.80 8.00 8.20 8.40 8.60 27 m/ z 44.95 16.18% .... 7.... !... 67 81 99 1 ' i ' ■ ' ' i ' ' ' ' I 1 1 1 1 I 1 1 1 1 I 1 1 ' 1 1 1 ' 1 1 1 1 ' ' ' i ' ' ' ' i ' 1 ' ' I 1 1 1 ' I 1 m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance 30 73 i 1 ' ■ ' i ‘ 7.80 8.00 ---PP 8.20 8.40 8.60 5000 m/ z 41.05 13.23% 44 58

15

m/z-> Abundance 10 20 30 40 50 60 70 #63573: 3-Pentanol, 3-methyi- 80

73 90 100 110 A, ........ ..... I. 7.80 8.00 8.20 8.40 8.60__ m/ z 39.05 9.97% i 5000 55 45 87 27 I , 39, | ' | I I I I | I I ! I ! m/z-> 10 20 30 40 50 60 70 80 90 100 110 ! 7.80 8.00 8.20 8.40 8.60

LB.D GCMS0208.M Mon Feb 11 12:34:10 2002 Page 1

NYC-WTC_000005165

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NYC-WTC_000005165Source: NYC Law Department, mirrored locally

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