GCMS sample results, AE00915, Feb 25, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\FEB1102\915.D Vial: 38 Acq On : 13 Feb 2002 12:08 am Operator: 209 GALOS Sample : GC/MS SCAN 1/14 FB Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.22 0.42 ug/1 31013 1,4-Dichlorobenzene-d4 12.35

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3 - Pentanol, /3-methyl - 102 C6H140 000077-74-7 9 2 3,4-Dimethyl-5-hexen-3-ol 128 C8H160 000000-00-0 9 3 2-Methyl-5/hexen-3-ol 114 C7H140 032815-70-6 9 4 Formic acid, ethyl ester 74 C3H602 1 00. 00 % 4 000109-94-4 m/z 73.00 Abundance Scan 346 (8.223 min): 915.D (-) 73

5000 43

57 87 7.80 8.00 8.20 8.40 8.60 ,35111/111,449 mHH +p Tr 103 m/z->_____ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105110 ■ |। ‘' I • ■ ‘' I ‘“ I “ 1 ‘ I " ' ‘ I ‘' m/z 43.05 44.54% Abundance #63573: 3-Pentanol, 3-methyl- 73

5000 i ■ • ■ ■ i • ■ 7.80 8.00 8.20 8.40 8.60 27 45 55 87 m/z 41.0,5 14.98% 1 39, nppt ’ 2- tpmpp 11.1.. 1111. i > l.. j.»J. I p-rrrp-rrTp-r miz->__ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance atc18: 4-90 pnp 46 73 _... A 43 7.80 8.00 8.20 8.40 8.60 5000 55 m/z 44.95 14.66%

27 67 81 99 .I.I..1.... J.... J.... 1.... 1I.... I.... III... M.... I. m/z-> 20_ 25 30 35 40 45 50 55 60 65 70 75 80 85 .90 95 100 105 110 Abundance #3017: 2-Methyl-5-hexen-3-ol }**’1**I* 73 7.80 8.00 8.20 8.40 8.60 55 m/z 39.05 6.95% 43 5000

27 V ' ‘11 ‘1 ‘ t ‘ 141+2421444411 miz->___ 20.25 30 35 40 45 50 55 60 65 79 75 80 8590.95 100 105 110 L I,....p...।....।......... ।.... ।.... ।.. i ' 1 1 ■ r1 1 ■ ' f ‘ 7.80 8.00 8.20 ‘ ‘ I ' ‘ ‘ ‘ I ‘ ' 8.40 8.60

915.D GCMS0208.M Wed Feb 20 09:54:07 2002 Page 1

NYC-WTC_000009510