GCMS analysis report for sample AE01230, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB1502\1230.D Vial: 37 Acq On : 17 Feb 2002 4:16 am Operator: 209 GALOS Sample : gc/ms scan 1/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.21 0.27 ug/1 24952 1,4-Dichlorobenzene-d4 12.33

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-PentanoV, 3-methyl- 102 C6H140 000077-74-7 25 2 2-Methyl -5-hexen-3-ol 114 C7H140 032815-70-6 23 3 Silane, tetramethyl- 88 C4H12Si 000075-76-3 23 4 3-HexanOl, 2,4-dimethyl- 130 C8H180 013432-25-2 9 Abundance Scan 345 (8.210 min): 1230.D (-) m/z. 73.00. 100.00% 713

5000 43

i 1 • ‘ ■ i • ■ ' ■ i ' ■ ■ ' i ' ■ ■ ' i ■ ' 87 7.80 8.00 8.20 8.40 8.60 m/z-> ■ ' i ■ ■ ■ ■ i • ■ ■ ■ i ■ 10 20 30 .. 1111,49.57,01a, 40 50 60 70 ' ‘ • i • '

80 i ■ ■ ■ ■ i

90 100 103 ' i ■

110 m/ z 43.0.5 48.05% Abundance #63572: 3-Pentanol, 3-methyl- 73

5000 _ A----------- 55 7.80_ 800 8-20 8.40 8.60 45 87 m/z 45.05 15.24% 27 ’*11*’1***I’*’I****1*1*’I’ -’I4 1 ■ ■ i ■ 1 11

m/z-> Abundance 10 20 30 40 50 60 70 80 90 100 110 73 55 7.80 8.00 8.20 8.40 8.60 43 5000 rn/z 40.95 13.84% 27 ..................... .................................................... .. , 81.................. miz->___ 10 . 20_ _ 30_ 40___ 50___ 60 70___ 80___ 90___ 100__ 110 Abundance #62932: Silane, tetramethyl- 73 7.80 8.00 8.20 8.40 8.60 m/z 39.0,5 12.10%

5000

45 ' ' i ‘ 15 ‘ i ‘ , ,1 ‘ i • ■ • ' i ' 1 1 ‘ i 53 59 ' ' 1 ' 1 1 ........... 88................................ ...... 11. . , , m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40 8.60

1230.D GCMS0208.M Thu Feb 21 09:30:35 2002 Page 1

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