GCMS sample results, AE00899, Feb 26, 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB1102\899.D Vial: 34 Acq On : 12 Feb 2002 8:15 pm Operator: 209 GALOS Sample : GC/MS SCAN 1/14 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

8.22 0.38 ug/1 30971 1,4-Dichlorobenzene-d4 12.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3 - Pentanoy, 3 -methyl - 102 C6H140 000077-74-7 33 2 Silane, tetramethyl- 88 C4H12Si 000075-76-3 25 3 2-Methyl/5-hexen-3-ol 114 C7H14O 032815-70-6 23 4 Pentane/ 3-methoxy-_ ___________ ___ 102“ C6H140 036839-67-5 9 Abundance Scan 346 (8.221 min): 899.D (-) m/z 73.00 100.00% 73

5000 43

r1 III’144*’I 51 55 59 5 69, 87 TTTTNNTTTTTI 11 ■ ■ ■ ■ i' ■ ■ ‘ 1'1 ■' i ■'' ‘ i' * 7.80 m/z 8.00 43.05 8.20 8.40 8.60 46.09%

J m/z->__ 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80.. 85 90 95 Abundance #63572: 3-Pentanoi, 3-methyi- 73

5000 1*‘**I‘*I* *"Tl i i i । [ । i 55 7.80 8.00 8.20 8.40 8.60 45 87 m/z 45.05 15.39% 27 31 42 69 84 [ ,59 1 “ ” 1111 ‘ I Tm TT T +mmmmmm m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance 093 s 73 M.,..... 7.80 8.00 8.20 8.40 8.60 5000 rn/z 41.05 14.13% 45 15 42 53 59 88 TOIIUpuammmn)Um2*0*mmPagum ■ ■ i'' “ I ■ ■ “ i “ ■' i •1 ‘' l1 ■" i ■

m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #3017:2-Methyl-5-hexen-3-ol .................... 73 7.80 8.00 8.20 8.40 8.60 55 m/z 39.05 18.33% 43 5000 27 31

m/z-> mkmm ■ ■ ‘ i'" ■ i " “ i “ “ i' U....111170a ’,1""33990111 ...... 81....................... 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 —3001"6""1"T 7.80 8.00 8.20 8.40 8.60

899.D GCMS0208.M Wed Feb 20 09:53:17 2002 Page 1

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