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GCMS analysis report for sample AE01220, Feb 2002

Machine-extracted title · confidence 95%

Analytical results page for sample AE01220 processed on February 25, 2002, showing surrogate recovery data.

NYC-WTC_000009721–000009729

Folder label: “GCMS X 1/17/02 A 2/17/02

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Scanned page image, NYC-WTC_000009728
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C: \HPCHEM\ 1 \DATA\ FEB1502122 0 . D Vial: 36 Acq On : 17 Feb 2002 3:18 am Operator: 209 GALOS Sample : gc/ms scan 1/17 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ******************************************************************** * Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.21 0.33 ug/1 29544 1,4-Dichlorobenzene-d4 12.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 33 2 Silane/ tetramethyl- 88 C4H12Si 000075-76-3 28 3 2-Methyl-5-hexen-3-ol 114 C7H140 032815-70-6 25 4 2-Butanone, 3-methoxy-3-methyl- 116 C6H1202 _036687-98-6 9 Abundance Scan 345 (8.213 min): 1220.D (-) m/z 73.00 100.00% 73

5000 43 !1/*/1/*/1/17/*/1/1///11//1/t//r5 —B, 7.80 8.00 8.20 8.40 8.60 • ' i ■ ■ ■ ■ i ■ ' ' ' i ■ ,1 ,1 1] 1 ..... . ' | 1 1 । 1 r1 1 1 1 i 1 1 1 1 1 1 L 87 ■ i ■ ■ ■ ■ i • ‘ 103 ‘ i ■ 1 ‘ ' i ■ m/z 43.05 38.45% miz-> 10.. 20___ 30... 40___ 50 . 60 70 __ 80___ 90 .. 100.. 110 Abundance #63572: 3-Pentanol, 3-methyl- 70

5000 —PAr 55 7.80 8.00 8.20 8.40 8.60 45 87 m/ z 41.0.5 16.51% 27 1 1—I_ pi , 1 ■ 1, 1 , t | 11 t r ■‘■I nni l > > | • l. . । ... i | ■ i i । | r m/z->10.. 20........ ... 30 40 50.. 60 70 80 90 100 110 Abundance • ■ . 73 ............... 1*’*I’*’’I1**’I’***I* \ A............... 7.80 8.00 8.20 8.40 8.60 5000 m/z 45.05 14.52% 45 15 i 53 59 88 'm/z~> Abundance 4*1/****I****I***1*A**1*I1III1IIII 10 20 30 40 50 60 70 #3017:2-Methyl-5-hexen-3-ol 80 __ 90 _ 100

73 ....... 110 A 7.80 8.00 8.20 8.40 8.60 55 m/z 39.05 8.57% 43 5000 27 — ‘ l 1I--— 181............... 11 T' 1 1 1 1 1 1 ' 1 ' ‘ I ‘ ' I ' ' m/z~> 10 20 30 40 50 60 70 80 90 100 110 7.80 8.00 8.20 8.40 8.60

1220.D GCMS0208.M Thu Feb 21 09:27:36 2002 Page 1

NYC-WTC_000009728

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NYC-WTC_000009728Source: NYC Law Department, mirrored locally

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