GCMS analysis results for sample AD31662, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\FEB1302\31662.D Vial: 6 Acq On : 13 Feb 2002 8:05 pm Operator: 209 GALOS Sample : GC/MS SCAN 2/11 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Pentanol, 3-methyl- Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.22 0.30 ug/1 29937 1,4-Dichlorobenzene-d4 12.34

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 3-Pentanol, 3-methyl- 102 C6H140 000077-74-7 36 2 2-Methyl-5-hexen-3-ol 114 C7H140 032815-70-6 25 3 3,4-Dimethyl/5-hexen-3-ol 128 C8H160 000000-00-0 9 4 1,3 -Dioxolane , 2-(3-bromo-5,5,5-tri 352 C10H16BrC13O2 000000-00-0 9 Abundance 7 Scan 346 (8.222 min): 31662.D (-) m/ z 73.0° 100 • 0 o % 73

5000 43 .. 7.80 8.00 8.20 8.40 8.60 I 49 55 87 103 TTT71111111117 I. I... I) 11111.1.111. .7). ■|. | ■ H, I ■ 1Pt i" ■' i ■"11 ■11 ■ i m/ z 43.0,5 43.19% miz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance #63573: 3-Pentanoi, 3-methyl- ’ 73

5000 i ■ ■ ■ ■ i 1 ■ 7.80 8.00 8.20 8.40 8.60 55 m/ z 45.0,5 15.97% 45 87 27 nmmm39 I TmTTTTT r ' " i' ‘" i HT ______ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 Abundance 73 55 7.80 8.00 8.20 8.40 8.60 43 5000 m/ z 41.05 12.70% 27 81 TIOONTTT m/z-> Abundance 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 #5018: 3,4-Dimethyl-5-hexen-3-ol 73 I‘ ‘II‘‘‘IIIISIII

7.80 8.00 LA 8.20 8.40 8.60 m/z 42.05 6.57% 43 5000 55

27 _ 67 mpt 81 99 ’ T 11" " i" ‘11 ■r" i" " I "111" ' ■ r ■" r ' m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 110 7.80 8.00 8.20 8.40 8.60

31662.D GCMS0208.M Fri Feb 15 10:12:14 2002 Page 1

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