GC/MS calibration results, PAH compounds, May 2002

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GC/MS instrument calibration report for polycyclic aromatic hydrocarbons and chlorinated compounds using 40 µg/L standards, dated May 2-3, 2002.

NYC-WTC_000045526–000045542

Folder label: “GCMS X 5/3/02 A 5/8/02”

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NYC 9/11 Public Portal Document

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Data File C:\HPCHEM\l\DATA\MAY0202\9451.D Vial: 10 Acq On 2 May 2002 11:38 pm Operator: Sample GC/MS SCAN 4/19 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 10 3,4-Dimethyl-5-hexen-3-ol Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

9.95 3.63 ug/1 328037 1,4-Dichlorobenzene-d4 12.20

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 3,4-Dimethyl-5-hexen-3-ol 128 C8H160 000000-00-0 9 2 3,5-Dimethyl-5-hexen-3-ol 128 C8H160 000000-00-0 9 3 Acetamide, N-methyl- 73 C3H7NO 000079-16-3 7 4 2-Methyl-5-hexen-3-ol____________ 114 C7H140 032815-70-6 7 Abundance 7 Scan 535 (9.945 min): 9451 .D (-) m/ z 73.10 100.00% 73

5000 43 57 139 1TT 0111 1‘ 1 ' i I.mmmmT"I 153 9.60 9.80 10.00 10.20 , 81 93 m/z->____ 10 20 30 361/59 —4— TTTTT 109 123 m/z i1 ’ r 11' 1 p 11 1 * 1 11 11 ■ ■ । 40 50 60 70 80 90 100 110 120 130 140 150 160 i i । 11 1 Tr 43.05 44 .46% Abundance #5018: 3,4-Dimethyl-5-hexen-3-ol 73

43 5000 55 I I I I I I I I I "1 11111 I" T c l ।1 9.60 9.80 10.00 10.20 m/ z 57.10 35.06% 27 ......I... 1. 1 i । i । i i । i i । i l i n । n n । । । । Ui tt —81—7 T 99 I ' ' 1 1 I । ■ ■ ■ ■ । ■ ■ ■ ■ । 11 m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #5017: 3,5-Dimethyl-5-hexen-3-ol 73 43 ‘11" R—mmn—TT 9.60 9.80 10.00 10.20 5000 55 m/ z 55.10 34.76%

27 | 81 99 1■।■'111' ■'' I'1111 ■ ■ ■ ■ ।11 TIUmuPumnunDmT 1111'1 r ........................................................ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #62528: Acetamide, N-methyl- 43 73 9.60 9.80 10.00 10.20 30 m/z 139.00 26.88%I 58 5000

--- T i1111111111'11111 i 11 11 r '1 11 11 1 ' i ■ । ■ ■ ■ ■ । • - ■ ■ । ■ _______ m/z-> 10 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 9.60 9.80 10.00 10.20

9451.D GCMS0501.M Fri May 03 08:42:21 2002 Page 10

NYC-WTC_000045540

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