GC/MS calibration results, PAH compounds, May 2002

Machine-extracted title · confidence 85%

GC/MS instrument calibration report for polycyclic aromatic hydrocarbons and chlorinated compounds using 40 µg/L standards, dated May 2-3, 2002.

NYC-WTC_000045526–000045542

Folder label: “GCMS X 5/3/02 A 5/8/02”

Page image

OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\MAY0 2 0 2\94 51.D Vial: 10 Acq On 2 May 2002 11:38 pm Operator: Sample GC/MS SCAN 4/19 Inst : 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0501.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 11 Butane, 1,3-dibromo-3-methyl- Concentration Rank 10 R.T. EstConc Area Relative to ISTD R.T. 11.60 1.09 ug/1 98541 1,4-Dichlorobenzene-d4 12.20 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Butane, 1,3-dibromo-3-methyl- 228 C5H10Br2 024443-15-0 25 2 Benzaldehyde, 4-methoxy-, oxime 151 C8H9NO2 003235-04-9 9 3 6H-Purin-6-one, 2-amino-1,7-dihydro 151 C5H5N5O 000073-40-5 9 4 Benzothiazole, 2-methyl- 149 C8H7NS 000120-75-2 9 Abundance Scan 716 (11.604 min): 9451 D (-) m/z 41.05 100.00% 41

69 149 5000 55 I ' 1 1 M । . . , । । । । । । — 81 109123 281 11.20 11.40 11.60 11.80 12.00 - "I i h i i i j 1 । 1'i'i r i-i i । i i m/z 69.05 65.60% m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #29403: Butane, 1,3-dibromo-3-methyl- 41 69

149 5000 i ' 1 1 1 i 1-4 1 1 1 1 11.20 11.40 11.60 11.80 12.00 27 53 m/z 149.05 55.36% 82 95 107 123135 i 1 ■1 ■ । •'r' i ■ 1 1 1 T 1 * 1 1 । 1 1 1 1 । 1 1 ‘TTUT i i । i > i i । i i n [ । । i । । । । i i । i i i i |""i ■ i” r i । i r m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #9998: Benzaldehyde, 4-methoxy-, oxime 1$1 i r ' ' 1 i i 1 1 1 1 i ' 1 11.20 11.40 11.60 11.80 12.00 5000 m/z 150.95 54.72% 108

134 77 m 92 I m/z-> Abundance 20 40 60 80 100120 140 160 180 200 220 240 260 280 #66826: 6H-Purin-6-one, 2-amino-1,7-dihydro- 1$1 .. n... । । । । । ] ' । । 1 । । । । । । । । i । । j r 11.20 11.40 11.60 11.80 12.00 m/z39.00 35.99% fl 5000 44

27 109 69 81 134 I I........ ......... li .. t- I ■ i 1 ■ • ■ i > ■ ■ ■ i ■ ■ - ■ । ■ ■ • ’ । — , i— — 1 1 ' i ' 1 1 1 i — 111'1' ।1 ■ I । । । > I ' । i 1 1 1 1 i 11 i 1 1 m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 11.20 11.40 11.60 11.80 12.00

9451.D GCMS0501.M Fri May 03 08:42:22 2002 Page 11

NYC-WTC_000045541

OCR can misread numbers and units. Confirm readings against the page image before using them.

NYC-WTC_000045541Source: NYC Law Department, mirrored locally

Related records

Browse subjects →

Ranked by indexed similarity. Reasons describe shared subjects and filing context; check the source records.

Same-box records

TCLP calibration table review document, April 2002 · Box DEP Box 25

NYC-WTC_000043238

Calibration data sheet listing retention times and response factors for deuterated internal standards used in TCLP testing.

1 shared topics · Same agency, volume and box · similarity 0.991