GCMS analysis results for sample AE01687, March 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB2 502\1687.D Vial: 8 Acq On : 25 Feb 2002 6:24 pm Operator: Sample : gc/ms scan 1/25 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L

Peak Number 1 2-Methyl-5-hexen-3-ol Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

8.19 0.28 ug/1 19431 1,4-Dichlorobenzene-d4 12.32

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Methyl-5-hexen-3-ol 114 C7H140 032815-70-6 23 2 N-Ethylformamide 73 C3H7NO 000627-45-2 5 3 Formic acid, ethyl ester 74 C3H602 000109-94-4 5 4 1,3-Di oxol Abundance / ane Scan 343 (8.195 min): 1687.D (-) 74 C3H6O2 000646-06-0 4 73.00... 100.00% i m/z 73

5000 43

39 47 51 87 57 69. 7.80 8.00 8.20 8.40 8.60 11] '' i " ■' i " ' ■ i' ‘ " i " " i " ■ ■ i ■ ■ ■ ‘ i'1 11' ’ " i " " I'1111'1111"11111 m/z 43.05 34.26% m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95

4 Abundance #3017:2-Methyl-5-hexen-3-ol 73 55 43 5000 7.80 8.00 8.20 8.40 8.60 27 m/ z 41.05 13.68%

m/z-> 5 ....... 31... J.. „ ' ■" i ■ ■ ■ ■ i " " 111111111 iT‛1 111 ■ “ ■ i ■" 11'11' 11111 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 70 ■ ■ “ I ■1 “ i ■'" i “ + A Abundance 30 73 7.80 8.00 8.20 8.40 8.60 5000 m/z 44.95 11.50% 44 58 27 15 41 12111111-1-11111111111110137010021110/01m1202‘11‘1‘10110"IIIT_uirt m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #62551: Formic acid, ethyl ester 29 7.80 8.00 8.20 8.40 8.60 m/Z 71.00 8.79% 5000 45

26 74 ' _. _ i ....... 42 1 m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 7.80 8.00 8.20 8.40 8.60

1687.D GCMS0208.M Thu Feb 28 09:31:30 2002 Page 1

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