GCMS analysis results for sample AE00006, Feb 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\FEB1302\6.D Vial: 8 Acq On : 13 Feb 2002 10:01 pm Operator: 209 GALOS Sample : GC/MS SCAN 2/11 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1,3-Dioxolane Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

8.22 0.28 ug/1 24882 1,4-Dichlorobenzene-d4 12.35

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,3-Dioxolane 74 C3H602 000646-06-0 5 2 Formamide, N,N-dimethyl- 73 C3H7NO 000068-12-2 4 3 N-Ethylformamide 73 C3H7NO 000627-45-2 4 4 2-Methyl-5-hexen-3-ol 032815-70-6 Abundance 7 Scan 346 (8.224 min): 6.D (-) 114 C7H140 m/ z 73.00... 100.00% 4 73

5000 43 -- i > ■ ■ ■ i ■ ■ 39. 51 55 7.80 8.00 8.20 8.40 8.60 mT H ----- 69. , 86 11 > ■ ■ ■ । ■ i' ■ • ■ । ■ ■ > ■ । m/ z 43.05 . 40.89% m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #62556: 1,3-Dioxolane 73

5000- 44 i ■ • ' 1 i ■ ■ ■ ■ i ■ ■ ■ ' i ■ ‘ ■ i ■ '

29 8.00 8.20 8.40 8.60 7.80 15 m/z 45.05 15.78% I 19 TITTTT " i" ■ ■ i" " ।।'11" h ■ ■ ■ ■ i ■" ‘ i ■ ■" i " " i

m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance ' . aroii . , . 44 73 ....... 7.80 8.00 8.20 8.40 8.60 5000 m/ z 41.0.5 12.38% 30 15 27 41 58 38 y ’l’’’’I—-tA1’*’*4+***N***’A’’I’I’’’’I’’I’III’SSSSIIIGC**IAAI’C’SL*| m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 Abundance #292: N-Ethylformamide 30 7.80 8.00 8.20 8.40 8.60 73 m/z 71.00 9.17% 5000 44 58 27

m/z-> 5 10 15 HTT THT —4 ' l1" ' i " ' i " " i " " i " TT 15 20 25 30 35 40 45i 50 55 60 65 70 75 80 85 90 7.80 8.00 8.20 8.40 8.60

6.D GCMS0208.M Fri Feb 15 10:13:40 2002 Page 1

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