GCMS analysis report for sample AE01231, Feb 2002

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\FEB1802\1231.D Vial: 38 Acq On : 18 Feb 2002 2:10 pm Operator: 209 GALOS Sample : gc/ms scan 1/17 Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 1,3-Dioxolane Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

8.21 0.32 ug/1 20146 1,4-Dichlorobenzene-d4 12.33

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 1,3-Dioxolane 74 C3H602 000646-06-0 7 2 Formamide, / N,N-dimethyl- 73 C3H7NO 000068-12-2 5 3 N-Ethylformamide 73 C3H7NO 000627-45-2 5 4 1-Pentanamine 87 C5H13N 000110-58-7_5 Abundance / Scan 345 (8.207 min): 1231 .D (-) m/z 73.00 100.00% 73

5000 43

51 69 7.80 8.00 8.20 8.40 8.60 39 I ।11 < • * * i ■" • । 87 m/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 >i*■।*>**।** m/z 42.95 28.17% Abundance #320:1,3-Dioxolane 73

5000 29 44 . M. / 7.80 8.00 8.20 8.40 8.60 m/z 40.95 11.67%

m/z->__ 5 ‘ ■ i11 ■ ■ i ■ ■ ‘ ■ i" " i +3+41 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 “ ।" “ । ■ ■ ■ ■ । • ■ । ■ ■ ■ ■ । • • 11 ■ ■ • 110—011010111071111

Abundance ’ .500T. .. 44 73 ■| 1 1 1 1 1 ' 1 ' 1 1 1 ‘ • i ■ • ■ ' i ■ ‘ 7.80 8.00 8.20 8.40 8.60 5000 m/z 44.95 11.65% 30 15 41 58 27 38 ’’271117-2*’1:H111121121111111030111201’00113111—o3TTTT1901T097 m/z-> Abundance 5 10 15. 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 30 #292: N-Ethylformamide N. Ill.... 7.80 8.00 8.20 8.40 8.60 73 m/z 71.00 7.85% 5000- 44 58 27 4 m/z-> 5i p 15

10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 7.80 8.00 8.20 8.40 8.60

1231.D GCMS0208.M Thu Feb 21 09:33:05 2002 Page 1

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