NYC-WTC_000009466
Gas chromatography mass spectrometry results for sample AE00899 analyzed on February 26, 2002.
Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Document / 13 pages
GCMS analysis report for sample AE01231, Feb 2002
Machine-extracted title · confidence 95%Analytical results page for sample AE01231 processed on February 25, 2002, showing surrogate recovery data.
NYC-WTC_000009773–000009785Folder label: “GCMS X 1/17/02 A 2/17/02”
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NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C: \HPCHEM\ 1 \DATA\ FEB18021231.D Vial: 38 Acq On : 18 Feb 2002 2:10 pm Operator: 209 GALOS Sample : gc/ms scan 1/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L
Peak Number 2 Cyclopentasiloxane, decamethyl Concentration Rank 3
R.T. EstConc Area Relative to ISTD R.T.
14.93 0.39 ug/1 31416 Naphthalene-d8 15.97
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 Cyclopentasiloxane, decamethyl- 370 C10H3005Si5 000541-02-6 78 2 N-(Trifluoroacetyl)-N,O,OO ’-tetr 553 C22H42F3NO4Si4 000000-00-0 37 3 Noradrenaline,/tetra-TMS 457 C20H43NO3Si4 000000-00-0 32 4 N - Me t hyl adrenal i ne, tri-TMS 413C19H39NO3Si3 000000-00-0 25 Abundance Scan 1077 (14.927 min): 1231.D (-) m/z 73.00 10O' . 00 % 73
5000 267 355
. 45 _____14.60 14.80 15.00 15.20 — — ——— 154 193 237 323 I m/z 266.90 45.02% m/z-2____ 50 100 150 200 250 300 350 400 450 500 550 Abundance #51266: Cyclopentasiloxane, decamethyl- 73
355 267 5000 ■ ■ i ■ ■ 1 ' I 1 1 1 1 I 14.60 14.80 15.00 15.20 m/z 355.05 38.55% 207 323 aass. m/z-> 50 100 150 200 250 300 350 400 450 500 550 Abundance 73 ■ ■ । ■ ■ ■ ■ ।(।1'1111'1 11 355 14.60 14.80 15.00 15.20 5000 m/ z 356.05 12.68%
45 147 193 267 538 m/z->___ 50__ 100. 150 __ 200 250 __ 300 __ 350 . 400 . 450.. 500 550 Abundance #57357: Noradrenaline, tetra-TMS............................................ 73 14.60 14.80 15.00 15.20 m/ z 268.00 12.11% 5000 102 355
45 147 442 ■ ‘I ■ ' m/z-> 50 100 150 200 250 300 350 400 450 500 550 14.60 14.80 15.00 15.20
1231.D GCMS0208.M Thu Feb 21 09:33:09 2002 Page 2
NYC-WTC_000009781
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NYC-WTC_000009781Source: NYC Law Department, mirrored locally
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