NYC-WTC_000009466
Gas chromatography mass spectrometry results for sample AE00899 analyzed on February 26, 2002.
Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Document / 13 pages
GCMS analysis report for sample AE01231, Feb 2002
Machine-extracted title · confidence 95%Analytical results page for sample AE01231 processed on February 25, 2002, showing surrogate recovery data.
NYC-WTC_000009773–000009785Folder label: “GCMS X 1/17/02 A 2/17/02”
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NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\FEB1802\1231.D Vial: 38 Acq On : 18 Feb 2002 2:10 pm Operator: 209 GALOS Sample : gc/ms scan 1/17 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS0208.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L
Peak Number 3 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
18.09 0.42 ug/1 34218 Naphthalene-d8 15.97
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 1,1,1,5,7,7,7-Heptamethy1-3,3-bis(t 444 C13H40O5Si6 038147-00-1 37 2 2H-1,4-Benzodiazepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 9 3 3-Trimethylsilyloxystearic acid, tr 444 C24H5203Si2 000000-00-0 9 4 Cyclohexasiloxane, dodecamethyl- 444 C12H3606Si6 ....... 000540-97-6 . 8 Abundance Scan 1421 (18.085 min): 1231 .D (-) m/z 73
5000 341 147 429
m/z-> 45 mmmpm L207 L1 L T‘1111121110110111101011111100111171111111111122221133801"T370"7"11 40 60 80 100120140160 180200 220240 260280 300 320340 360380400420 17.80 m/z 341.00 18.00 18.20 18.40 30.41% Abundance #56714:1,1,1,5,7,7,7-Heptamethyi-3,3-bis(trimethyisiioxyjt 73 147 ................ ....................... 5000 267 355 429 17.80 18.00 18.20 18.40 45 207 m/z 147.00 17.55% I" " i TOmpOma"Pan—mapmPP]T m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 Abundance 73 341
17.80 18.00 18.20 18.40 5000 m/z 429.0 11.04% 45 91 116 146 227 269 315 m/z->___40 60 80 100120140160 180200 220 240 260280300 320 340 360 380 400420 Abundance #56734:3-Trimethylsilyloxystearic acid, trimethylsilyl est 73 17.80 18.00 18.20 18.40 m/z 342.00 10.79% 5000 147 233
313 429
m/z-> 023937 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 400 420 17.80 18.00 18.20 18.40
1231.D GCMS0208.M Thu Feb 21 09:33:14 2002 Page 3
NYC-WTC_000009782
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NYC-WTC_000009782Source: NYC Law Department, mirrored locally
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