Large multi-page laboratory data sheet containing sample analysis results and metadata for DEP GCMS records from January to February 2002.
NYC-WTC_000004149–000004492Folder label: “GCMS X 12/18/01, 2/8/02 A 2/10/02, 1/10/02, 1/14/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2 701\30650.D Vial: 46 Acq On : 30 Dec 2001 3:26 am Operator: 209 GALOS Sample : GC/MS SCAN 12/18 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L
Peak Number 4 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T.
17.45 6.40 ug/1 3635200 Naphthalene-d8 15.28
Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 1,1,1,5,7,7,7-Heptamethy1-3,3-bis(t 444 C13H40O5Si6 038147-00-1 27 2 2H-1,4-Benzodiazepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 22 3 Silane, [1,2,3-benzenetriyltris (oxy 342 C15H30O3Si3 017864-23-2 10 4 Pregnane-3,20-dione, 11-[(trimethyl 462 C26H46N203Si 057305-27-8 9 Abundance Scan 1351 (17.448 min): 30650.D (-) m/ z 73.00 100.00% 73
5000
45 147 429 341 . ... n...... 17.20 17.40 17.60 17.80 0 "TT i 1197 117|.. “I'" " n | 179.. 207226 251 281 311 ( I "" I " " I'T', I,' TTT*—nuum)mm 367 397 I IT m/z 341.00 29.52% m/z-> 40 60 80 100J20140160180200 220240260280 300 320 340 360 380 400 420 Abundance #56714: 1,i,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxyjt 73
147 .................. ,........................ 5000 267 355 429 17.20 17.40 17.60 17.80 45 207 m/z 147.00 14.18%
m/z-> i" " i"1 ■ i" ■ * i1H ■ i TT" .............. j l.............. i11 ■1 r ■" i1"' i" *111'1 ■ i1 40 60 80 100120140160180200220240260280300320340360380400420 t 1’10100110001010010110111
Abundance 88 niod azopit-2-one 7- toro-1 3-dinydro 5- 73 341
17.20 17.40 17.60 17.80 5000 m/z 342.00 9.86% 45 91 227 269 3151 116 146
m/z--> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #73587: Silane, [1,2,3-benzenetriyltris(oxy)]tris[trimethyl- \, 1 1 ' 73 239 17.20 17.40 17.60 17.80 m/z 325.00 9.57% 342 5000
45 133 1 211 mmmm . m/z-> 40 60 80 100120140160180200220 240 260 280 300 320 340 360 380 400 420 17.20 17.40 17.60 17.80
30650.D GCMS1126.M Mon Jan 28 11:18:16 2002 Page 4
NYC-WTC_000004374
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28479 analyzed in early December 2001.
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Laboratory report detailing GCMS analysis of sample AD28269 conducted on November 30, 2001.
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Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
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Analytical commentary for sample AD28149 dated November 29, 2001, noting no unusual compounds but low recovery rates for LCS standards.
1 shared non-person entities · 1 shared topics · similarity 0.996
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Laboratory analyst notes on GCMS scan results and recovery rates for sample AD28666 analyzed in early December 2001.
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NYC-WTC_000004148
Fragmented OCR text showing dates and identifiers for a DEP GCMS record dated February 2002.
Filed in the same folder
NYC-WTC_000036712
GCMS analysis report for sample AD29563 listing unknown compounds and surrogate recovery data from January 28, 2002.
Similar indexed content
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