Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30357 conducted on January 10, 2002.
NYC-WTC_000017748–000017769Folder label: “GCMS X 12/13/01 A 12/27/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\DEC2701\30357.D Vial: 18 Acq On : 28 Dec 2001 4:40 am Operator: 209 GALOS Sample : GC/MS SCAN 12/13 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 1,1,1,5,7,7,7-Heptamethyl-3,3- Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 17.45 4.35 ug/1 1739020 Naphthalene-d8 15.28 Hit# of 5 Tentative ID MW MolForm CAS# Qual
1 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H4005Si6 038147-00-1 16 2 2H-1,4-Benzodiazepin-2-one, 7-chlor 342 C18H19C1N2OSi 055299-24-6 12 3 Silane, [1,2,3-benzenetriyltris (oxy 342 C15H3003Si3 017864-23-2 10 4 Pregnane-3,20-dione, 11-[(trimethyl 462 C26H46N2O3Si 057305-27-8 9 Abundance Scan 1352 (17.453 min): 30357.D (-) m/z 73.00 100.00% 73
5000 341 147 429 45 , 17.20 17.40 17,60 17.80 i 117 [ 179 207225 251 281 311 L 1___ 397 97—mnmmm5n0mm1a2m000T 1—mn I “"i1” •।■■•■। । “i 11 • m/z 341.00 32.11% miz-> 40 60 80 100120140160180200220240260280300320340360380400420 'Abundance #56714:1,1,1.5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t 73 147 ................ M.................. I I I J J I I J I 13 J “ ! |' I J TT | I 1k 5000- 267 355 429 17.20 17.40 17.60 17.80 45 207 m/z 147.00 14.45% . ......................... I ..............,,J,...... TT TTTTp^TTpTT^p-rrrpTTTTm^rrrtTT^^ m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #48337: 2H-1 4-Benzodiazepin-2-one. 7-chiorg-1.3-dihydro-5- 73 341 1 1 i ■ ■ ■ ' f1 ■ 1 • i ■ ■ ■ ■ i ■ ■ 17.20 17.40 17.60 17.80 5000 m/z 342.00 10.65% 45 91 i 1 116 146 227 269 315 | I******)**** I ‘ ’ * • I ’ ’ •41 ’ ’'' I I . » . . I . I . . I . . < . I I . > H ..». l. . . « J . . . . I H . . I 1 1′1101-101200011108118 m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #48324: Silane, [1,2,3-benzenetriyltris(oxy)]tris[trimethyl- 73 17.20 17.40 17.60 17.80 m/z 325.00 10.45% 239 5000 342
45 TTT1’ 133, 179 211 TmNupTpgm ""i'"‘I । ii । ii314 L ________________ ।. । .> i ipi 111,,.. ।,.,, ।... 11,,.. 11 .........M........... .. । pi in 11 r 1111 > । m/z-> 40 60 80 100120140 160 180 200 220240 260 280 300 320 340 360 380 400 420 17.20 17.40 17.60 17.80
30357.D GCMS1126.M Wed Jan 02 11:00:18 2002 Page 5
NYC-WTC_000017759
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NYC-WTC_000017833
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30351 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017703
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30425 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017808
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30352 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019130
Laboratory report of gas chromatography-mass spectrometry analysis for sample AD30256 conducted on January 9, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017854
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30252 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017724
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30426 conducted on January 10, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017675
Laboratory report detailing gas chromatography-mass spectrometry analysis of sample AD30251 conducted on January 9, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018470
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018445
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018546
Laboratory report showing GC/MS calibration data for polycyclic aromatic hydrocarbons and deuterated standards.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036162
Laboratory report noting GCMS scan results for sample AD29231 with phthalates detected and low recovery requiring re-analysis.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000033911
Calibration data sheet recording response factors and retention times for standard compounds used in GCMS TCLP analysis on November 26-27, 2001.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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