GCMS analysis of environmental sample AD30118 conducted January 9, 2002.
NYC-WTC_000016783–000016794Folder label: “GCMS X 12/12/01 A 12/19/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document Library Search Compound Report
Data File C: \HPCHEM\ 1 \DATA\JAN03 02\30118.D Vial: 11 Acq On 3 Jan 2002 8:20 pm Operator: 209 GALOS Sample gems scan 12/12 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 1,1,1,5,7,7,7 -Heptamethyl-3,3- Concentration Rank 4
R.T. EstConc Area Relative to ISTD R.T.
17.31 0.56 ug/1 205232 Naphthalene-d8 15.12
Hit# Of 5 Tentati ID MW MolForm CAS# Qual
1 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5S16 038147-00-1 35 2 2H-1,4-Benzodiazepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 9 3 Silane, [1.2, 3-benzenetriyltris (oxy 342 C15H30O3Si3 017864-23-2 9 4 Pregnan <3,20-dione, 11-[(trimethyl 462 C26H46N2O3Si 057305-27-8 9 Abundance ............ Scan 1336 (17.306 mln): 30118.D (-) m/ z 73.0.0 100.00% 73
5000
45 147 341 429 1 L 17.00 17.20 17.40 17.60 1 ’1 1 117 [ 179.207 ‘ *1—l——00t—001088811 . 251 311 1 1 111 h l“| Hf ij in i ji h I] i i'f» | ih i j m rj i rtq|71111«। ।«j n ।«। r«1111 < 11111 < 1111111 r< m/z 341.00 29.75% m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bls(trtmethylsiloxy)t 73
147 5000 267 355 429 ‘ 17.00 17.20 17.40 17.60 ' ‘ ‘ 45 207 m/z 147.00 14.61% i m/z-> H Th . 1.... 1.... f.. .11... .j.... 1.... I. 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #48337: 2H-1,4-Benzodiazepin-2-one. 7-chloro-1.3-dihydro-5- 73 341 / 17.00 17.20 17.40 17.60 ‘ ‘ 5000 m/z 324.90 10.77% 45 91 I I 116 146 227 269 315 mmmppmpmp ! TTTmgp m/z-> Abundance ‘'1 • I ’ * ’ TrTTTp-rrTpTrrjTTTTpTTT^^ 40 60 80 100120140160180200220240260280300320340360380400420 #73587: Silane, [1,2,3-benzenetriyltris(oxy)]tris[trimethyl- , ......... \.................... 73 239 17*00 17.20 17.40 17.60 m/z 429.05 9.68% 342 5000
45 133
miz-> ।.... j.... (..z.I । . 211 3 unpiup.iiiu TT|.|p I n |. 40 60 80 100120140160180200220240260280300320340360380400420 mm 1 1 i 1 ■ • ‘ i ■ ■ ■ ■ n 17.00 17.20 17.40 17.60 1 1 i 1 1 1 1 i
30118.D GCMS0103.M Mon Jan 07 10:36:44 2002 Page 3
NYC-WTC_000016792
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NYC-WTC_000018983
GCMS analysis report for sample AD31135 showing detection of unknown compounds and surrogate recovery data from February 11, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018142
Automated laboratory log recording GCMS analysis of sample AD30711 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017969
Laboratory report documenting GCMS analysis of sample AD30473 conducted on January 24, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017958
Laboratory report documenting GCMS analysis of sample AD30489 conducted on January 24, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000017097
Laboratory report detailing GCMS analysis of sample AD30486 including DDD surrogates on January 18, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000019004
GCMS analysis report for sample AD31130 showing detection of unknown compounds and surrogate recovery data from February 11, 2002.
1 shared topics · Same agency, volume and box · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018238
Gas chromatography-mass spectrometry analysis of sample AD30983 performed on 1/25/02, detecting 2,4-DDD compound at 101 micrograms with 5.0 MDL.
1 shared topics · Same agency, volume and box · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049734
GCMS analysis report for sample AD31642 conducted on February 11, 2002.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049762
GCMS analysis report for sample AD31640 conducted on February 11, 2002.
1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049851
Laboratory report showing GCMS analysis of sample AD29519 including unknown compounds and surrogate recovery data.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036831
Gas chromatography-mass spectrometry analysis of sample AD29666 identifying unknown compounds and surrogate recovery data (2,4-DDD at 72%), January 28, 2002.
1 shared topics · similarity 0.997
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000049723
GCMS analysis report for sample AD31632 conducted on February 11, 2002.
1 shared topics · similarity 0.996
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000016680
Document header or index page associated with gas chromatography mass spectrometry records from December 2001.
Filed in the same folder
NYC-WTC_000016681
Method blank report confirming absence of contamination during volatile organic compound testing procedures in January 2002.
Filed in the same folder
NYC-WTC_000016689
GCMS calibration report listing target compounds and response factors for December 2001 analysis.
Filed in the same folder
NYC-WTC_000016694
Reference standard analysis report verifying instrument performance for volatile organic compound testing in early 2002.
Filed in the same folder
NYC-WTC_000016699
GCMS analysis of environmental sample AD30021 conducted January 9, 2002.
Filed in the same folder