Automated laboratory log recording GCMS analysis of sample AD30714 including detection of unknown compounds and surrogates.
NYC-WTC_000018174–000018193Folder label: “GCMS X 12/27/01 A 1/16/02”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File C:\HPCHEM\1\DATA\DEC3101\30714.D Vial: 29 Acq On 1 Jan 2002 4:05 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2H-1,4-Benzodiazepin-2-one, 7- Concentration Rank 1
R.T. EstConc Area Relative to ISTD R.T. 17.45 3.95 ug/1 1317590 Naphthalene-d8 15.28 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2H-1,4-Benzodiazepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 22 2 Silane, [1,2,3-benzenetriyltris (oxy 342 C15H30O3Si3 017864-23-2 12 3 1,1,1,5,71,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 12 4 3-Trimeth Abundance ylsilyloxystearic acid, tr 444 C24H5203Si2 Scan 1352 (17.455 min): 30714.D (-) 000000-00-0 9 m/z 72.9.5 100.00% 73
5000 341 . . । . I . . i . । . . . . । . 147 429 17.20 17.40 17.60 17.80
miz-> ttk45 117 [ 179 207225 251 281 311 1 | ITTNIETara TPnepm 40 60 80 100120140160180200220240260280300320340360380400420 397 . TTTTTpTrryTrtTp- m/z 341.00 31.13% Abundance #48337:2H-1.4-Benzodiazepin-2-one, 7-chloro-1,3-dihydro-5- 73 341
5000 ...................... 17.20 17.40 17.60 17.80 45 91 m/z 147.00 14.18% j 116 146 227 269 315............. . mfe-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #48324: Silane, [1 2.3-benzenetriyltris(oxyi]tris[trimethyl- 73 _____________ k_____________ tdd,B///*/*//*/n/m/2//no/1/B.k.n. 239 17.20 17.40 17.60 17.80 5000 342 m/z 342.00 10.59% 45 133 179 211 . ._________________ TTppOpp >.314 • • ■ l. ■•H■'''1' •'11" ■. pl. < j l. ■. j.. . IJ ll 111 ■ > 1111 miz-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t - 73 17.20 17.40 17.60 17.80 m/z 325.00 10.38% 147 5000 267 355 429 45 207
‘ ‘1‘444 J...... I...... Ti..... .1 .। f...I(।A.।. ‘ • i 1 1 miz-> 40 60 80 100120140160180200220240260280300320340360380400420 17.20 17.40 17.60 17.80
30714.D GCMS1126.M Wed Jan 23 08:50:03 2002 Page 4 NYC-WTC_000018184
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NYC-WTC_000018155
Automated laboratory log recording GCMS analysis of sample AD30713 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018733
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30934 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018754
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30935 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018262
Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018693
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30909 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018664
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30907 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018214
Automated laboratory log recording GCMS analysis of sample AD30712 including detection of unknown compounds and surrogates.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018194
Automated laboratory log recording GCMS analysis of sample AD30605 including detection of unknown compounds and surrogates.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018716
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30933 conducted on January 28, 2002.
1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000018605
Laboratory report documenting gas chromatography mass spectrometry results for sample AD30705 conducted on January 28, 2002.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000016096
GCMS analysis report for sample AD27288 showing surrogate recovery and unknown compounds from December 19, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000036656
Laboratory comments on GCMS scan results for sample AD29517 noting low recovery and scheduling re-extraction.
1 shared non-person entities · 1 shared topics · similarity 0.998
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000018058
Document with unreadable text from the GCMS X folder series in DEP Box 16.
Filed in the same folder
NYC-WTC_000018059
Calibration verification report using DFTPP standard for GCMS instrument performance check on January 1, 2002.
Filed in the same folder
NYC-WTC_000018060
Laboratory report documenting GCMS calibration analysis of sample AD30694 conducted on January 18, 2002.
Filed in the same folder
NYC-WTC_000018064
Reference data table listing response factors and concentrations for organic compounds used in GCMS analysis of sample AD30694.
Filed in the same folder
NYC-WTC_000018069
Blank analysis report showing non-detectable levels of target organic compounds in sample AD30694.
Filed in the same folder