NYC-WTC_000018262
Laboratory report documenting GCMS analysis of sample AD30985 conducted on January 25, 2002.
1 shared topics · Same agency, volume and box · similarity 0.995
machine-extracted · confidence unavailable · Check page ↗Document / 17 pages
GC/MS blank analysis results, Jan 25 2002
Machine-extracted title · confidence 100%Laboratory report showing non-detect results for volatile organic compounds in a GC/MS blank sample.
NYC-WTC_000018588–000018604Folder label: “GCMS X 12/19/01 A 1/2/02”
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NYC 9/11 Public Portal Document Library Search Compound Report
Data File C:\HPCHEM\l\DATA\DEC3101\LBE.D Vial: 40 Acq On 2 Jan 2002 2:43 am Operator: 209 GALOS Sample gems scan 12/19a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2H-1,4-Benzodiazepin-2-one, 7- Concentration Rank 2
R.T. EstConc Area Relative to ISTD R.T.
17.45 2.24 ug/1 919355 Naphthalene-d8 15.28
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2H-1,4-Benzodiazepin-2-one, 7-chlor 342 C18H19ClN2OSi 055299-24-6 22 2 3-Trimethylsilyloxystearic acid, tr 444 C24H5203Si2 000000-00-0 17 3 1,1,1,5,7,7,7-Heptamethyl-3,3-bis(t 444 C13H40O5Si6 038147-00-1 16 4 Silane, [1,^<3-benzenetriyltris(oxy 342 C15H30O3Si3 017864-23-2 10 Abundance Scan 1352 (17.453 min): LBE.D (-) m/z 73.0.0 100.00% 73
5000 341 ............................................... 147 429 . 45 17.20 17.40 17.60 17.80 117. [ 179.207225 251 281 311 l t 397..... L m/z-> oW p-rTrp-rn-pTTTp- 40 60 80 100120140160180200220240260280300320340360380400420 m/z 341.00 28.50% Abundance #48337:2H-1,4-Benzodiazepin-2-one, 7-chloro-1,3-dihydro-5- 73 341
5000 17.20 17.40 17.60 17.80 45 m/z 147.00 14.21% 91 116 146 227 269 315 It _______________।. TWg TIWITIIaaga) ]..., pT. ip. >.p miz-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #56/34: 3-Trimethylsilyloxystearic acid, trimethylsilyl est 73
17.20 17.40 17.60 17.80 147 233 m/z 325.00 9.59% 5000
313 429 189 | 339 387 mppmmmpmmm pTYrp-rn-p TCmmmn) 1 m/z-> 40 60 80 100120140160180200220240260280300320340360380400420 Abundance #56714:1,1,1,5,7,7,7-Heptamethyl-3,3-bis(trimethylsiloxy)t ■ ■ i ‘ 1 ■ ■ i ■ • ‘ ■ i ■ • • • i • ■ 73 17.20 17.40 17.60 17.80 m/z 342.00 9.51% 147 5000 267 355 429 45 207
m/z—> 4 mmm TTpTTTpTTrpTTT-prrr]- nhp TIPanp—me*g—mnu—T pn-rp-rrTp- 40 60 80 100120140160180200220240260280300320340360380400420 17.20 17.40 17.60 17.80
LBE.D GCMS1126.M Fri Jan 25 12:07:31 2002 Page 3
NYC-WTC_000018595
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