GCMS analysis log for sample AD30714, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\DEC3101\30714.D Vial: 29 Acq On 1 Jan 2002 4:05 pm Operator: 209 GALOS Sample gems scan 12/19 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Cyclopentasiloxane, decamethyl Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

14.31 2.69 ug/1 898625 Naphthalene-d8 15.28

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Cyclopent iloxane, decamethyl-. 370 C10H3005Si5 000541-02-6 50 2 Benzoic acid, 2,6-bis[(trimethylsil 370 C16H30O4Si3 003782-85-2 43 3 3,4-Dihydroxybenzyl alcohol,tris(tr 356 C16H3203Si3 068595-79-9 38 4 Benzeneacetic acid, .alpha.,4-bis[( 326 C15H26O4Si2 055334-40-2 37 Abundance 2 Scan 1009 (14.306 min): 30714.D (-) m/z 100.00% 73

5000 267 355 ‘ ‘ I ‘ * 1 ‘ I ' 1 ‘ ' I 45 , 251 14.00 14.20 14.40 14.60 , 89 108 133 154 177 193 223 i 0+ “ i'11 TPmppmgr ___ i TT .4. 293... 323339, 4.., m/z 267.00 33.00% miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51266: Cyclopentasiloxane, decamethyl- 73 355 267 5000 T T T T 1 14.00 14.20 14.40 14.60 m/z 355.05 24.66% . 191207 j 11»»‘l • ।1».»11.111».»11.». 11.». j ।»»»j r« * । j । i 111 > ।»»। • T •»I •»» 251 t .323339.1.., miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #51296: Benzoic acid. 2.6-bis(trimethylsi y joxyl- trimet 73 355 1 ■ i ■ ■ ■ ■ i ■ ■ ■ ■ I ■ ■ ■ ■ i ■ ■ ■ ‘ I 14.00 14.20 14.40 14.60 5000 ................... ; 9.00% 147 267 47 ! I 208 249 । 283 .< 1111... 11... I.... I. I.»I...»I TTmnuatuma-0 ——maa22 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 Abundance #49868: 3,4-Dihydroxybenzyl alcohol, tris(trimethylsilyl)- ■ ■ i ■ ■ ‘ • i • • • • i ■ ■ ■ • i ■ ■ ‘ ■ i 73 14.00 14.20 14.40 14.60 m/z 268.00 8.98% 267 5000 179 356 45 147 209 237 i i i । » i i j « i <» । i i » i । i i i i । • J I k j i i t « i ) I . . I . I . . I . . I <I . I . . ] . ’ 190111—312 0—2200’nT r i • • ■ ‘ i ‘ ■ i • ' ■ ' i ' 1 1 ■ i ■ ■ • ■ i ' ‘ • i m/z—> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 14.00 14.20 14.40 14.60

30714.D GCMS1126.M Wed Jan 23 08:49:58 2002 Page 3

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