GCMS analysis results for sample AD30118, Jan 2002

NYC 9/11 Public Portal Document Library Search Compound Report

Data File C: \HPCHEM\ 1 \DATA\JANO 302\30118.D Vial: 11 Acq On 3 Jan 2002 8:20 pm Operator: 209 GALOS Sample gems scan 12/12 Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Chrysene-dl2 Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

32.84 30.01 ug/1 5160500 Perylene-d12 36.91

Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 Chrysene-d12 001719-03-5 98 240 C18D12 2 Naphtho [2,1-b:7,8-b’]difuran, 1,2,9 240 C16H1602 068873-21-2 47 3 1,4-Bis(6-methylpyridyl-3)-butane 240 C16H20N2 000000-00-0 47 4 -Furo[2',3':4,5]oxazolo[3,2-a]pyr 240 C10H12N2O5 022423-26-3 43 Abundance Scan 3028 (32.839 mln): 30118.D (-) m/z 240.15 100.00% 21.0

5000

106 120

m/z "7 t i | I i i k i » I » j » i i i । i r 32.60 32.80 33.00 33.20 i 42 52: 66 78 92 TTHH—t 1—132146156 170180194 294222.4 252 ‘ ■ i 24.64% m/z-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #32068: Chrysene-d12 240

5000 1 ■ i ■ • ■ ■ i ■ • ■ ■ I1 1 1 1 1 1 1 32.60 32.80 33.00 33.20 m/z 239.15 23.31% 1 106 120 919 || ' ............................ 1. J,........ .. .................... ~. iill, m/z-> 40 60 80 100 120 140 160 180 200 220 240 TII Abundance #32043; Naphtho[2,1-b:7.8-bldifuran 1 2.9 10-tetrahydro-2 240 —P I ’ 1 1 1 1 1 1 32,60 32.80 33.00 33.20 5000 m/z 241.15 18.82% 211 152 181 197 225 ' ' i ‘ ■■1i■'■■i‘' i''■'i'‘'•i'‘1■i‘'■i ’ ■ ‘ ■ ■ i ' ■ • ' i‘ ‘ 'i ■ ■ ■ ■ i miz-> 40 60 80 100 120 140 160 180 200 220 240 Abundance #32046:1,4-Bis(6-methylpyrtdyl-3)-butane 1 ■ i ■ • ■ • । • ■ ■ ■ ।11111 ■ ■ 240 32.60 32.80 33.00 33.20 107 ■ " 17.12% 5000 77 120 134 39 51 65 | 92 rr ■ ■i' 1''i'■• 'i • • • • । • ■ ‘ i ■ ■ ' ‘ i ‘ ‘ ■ i ‘ ‘ i 1 ' ' ■ i ' ' TTT m/z-> 40 60 80 100 120 140 160 180 200 220 240 32.60 32.80 33.00 33.20

30118.D GCMS0103.M Mon Jan 07 10:36:48 2002 Page 4

NYC-WTC_000016793