GCMS analysis results, sample AD30315, Jan 2002

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC2101\30315.D Vial: 6 Acq On : 22 Dec 2001 11:44 am Operator: 209 GALOS Sample : gc/ms scan 12/13a Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\GCMS1126.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Perylene-dl2 Concentration Rank 2 R.T. E st Cone Area Relative to ISTD R.T. 37.11 13.88 ug/1 2746790 Chrysene-dl2 33.01 Hit# of Tentative ID MW MolForm CAS# Qual

1 Perylehe-dl2 264 C20D12 001520-96-3 94 2 4,6-Di (2-hydroxyphenyl)pyrimidine 264 C16H12N2O2 000000-00-0 47 3 Cycyoocta[1,2-b:4,3-b':5,6-b11:8,7- 264 C16H804 056598-42-6 45 \ )4 2-9bco-6-phenyl-4-(2-hydroxyphenyl) - 264 C16H12N2O2 000000-00-0 40 \ Abundam Scan 3493 (37.108 mln): 30315.D (-) m/z 264.10 100.00%

1 204

5000 132 ’ 1 I • ■ ’ • I 156168180194/208220232 252 40 52 64 76 88 102 118 । T——,dm"TMmgT 281 1** 36.80 37.00 37.20 37.40 m/z 263.10 44.99% m/z~> 40 60 80 100 120 140 160 180 200 220 240 260 280 Abundance #36687: Perylene-d12 264

5000 36.80 '37'60 37'20 37.40 ‘ ‘ m/z 132.00 26.11%

m/z-> . ........... 40 60 80 100 120 140 160 180 200 22 220 240 260 280 Abundance #36598:4.6-Di(2-hydroxyphenyl)pyrimidine 264 * 1 [1 1 • * • 1 I 36.80 37.00 37.20 37.40 5000 m/z 260.05 23.73% 34 100 236 171 ■ • । • i ■ ■ ■ ■ । ■ 208 221 248 I ‘ • 11 ■ ■ ■ ■ i ‘ ■ i ■ ' m/z-> 40 60 80 100 120 140 ' 160 " 180 " 200' 220 240 260 280 Abundance #36596: Cycloocta[1,2-b:4.3-b':5,6-b":8,7-b"']tetrafuran ‘ I' 1 ' i ■ ■ ' ■ i

234 264 36.80 37.00 37.20 37.40 m/z 130.00 22.60% 152 5000 208

—y 75 132 179 43 T .1 111 ■ ‘ •111 ■ ■11 •''111111111 • 1111 ■ 1 ■ 11 * 1 • ■11 • • ■ ■ i ■ ■ 7‘I4444t miz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 36.80 37.00 37.20 37.40

30315.D GCMS1126.M Wed Jan 02 10:19:28 2002 Page 3

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