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GC/MS analysis results for sample AD22578, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22578 conducted on October 10-11, 2001, identifying unknown compounds.

NYC-WTC_000087163–000087179

Folder label: “GC/MS Scan 9/19/01

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Scanned page image, NYC-WTC_000087177
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\SEP2801\22578.D Vial: 6 Acq On : 28 Sep 2001 5:19 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library :. C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 8 R(+)5,7-Dimethyl-l,6-octadiene Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 36.96 2.10 ug/1 300912 Perylene-dl2 37.28 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 R(+)5,7/oimethyl-l,6-octadiene 138 C10H18 000000-00-0 62 2 Ethancy, 2-(9-octadecenyloxy)-, (Z) 312 C20H40O21 005353-25-3 52 3 Bicyc/o[3.1.0]hexan-3-one, 4-methyl 152 C10H16O 001125-12-8 50 4 2(1H/-Naphthalenone, octahydro-4a-m 208 C14H24Q 054594-42-2 49 Abundance/ Scan 3477 (36.957 min): 22578.D (-) m/z 55.00 100.00% / 55 81

5000

T 31 36.60 36.80 37.00 37.20 qu 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 m/z 81705 78.32% Wsundance #7019: R(+)5,7-Dimethyl-1,6-octadiene 5 83

5000 36.60 36.80 37.00 37.20 Wz 69700 71723%

•nZz-> 40 '' I' ‘ Mi ^^138 ' I " "I' I'''' I'''' I'' ‘' I'''' I'''' I'''' I ‘ ‘' I'' ‘' I'''' I 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #44553: Ethanol, 2-(9-octadecenyloxy)-. (Z)- 55 8(2

36.60 36.80 37.00 37.20 5000 <7 m/z 67.00 68.60%

123 250 I 292 312 I " '' I I' • " I' "' I • ’ " I'' " I»' ” I I'' " I " '' I i'' " p ■nZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #10295: Bicyclo[3.1.0]hexan-3-one, 4-methyl-1-(1-methylethy T 81 110 36.60 36.80 37.00 37.20 m/z 83705 61.00% 5000

152 I'' I' I I' " • I" " I" " I I'' " I'' " I'' " I P Tl/Z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 se'eo se'so 37'00 37120

22578.D NP091101.M Wed Oct 03 11:30:11 2001 Page 8

NYC-WTC_000087177

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NYC-WTC_000087177Source: NYC Law Department, mirrored locally

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