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GC/MS analysis results for sample AD23322, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23322 conducted on October 15, 2001.

NYC-WTC_000088263–000088289

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088286
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23322.D Vial: 15 Acq On : 12 Oct 2001 3:48 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 17 Octacosane Concentration Rank 16 R.T. EstConc Area Relative to ISTD R.T. 38.36 0.47 ug/1 40291 Perylene-dl2 37.22 . Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Octacosape 394 C28H58 000630-02-4 53 2 Heptacjafsane 380 C27H56 000593-49-7 53 3 Hexat/riacontane 507 C36H74 000630-06-8 53 4 IQZMethylnonadecane______________ 282 C20H42 000000-00-0 53 'Xbunda^e Scan 3630 (38.363 min): 23322. D (-) “mTz 56.95 100.00% 57

5000 85 207

n/z-> Abundance iW u 40 60 113 253 281 I " " J«• " I " 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 #74211: Octacosane I .... I n-T. p . . . I 38.00 38.20 38.40 38.60 “mTz 43.05 72.68%

43

71 5000 38.00 38.20 38.40 38.60 m/z 71.00 70.67% i I , 127 155 183 211 I. I I «I rI 11 111 1 .1 1 11 I .■‘i I. .1 . I p I I'l . I rfp I'HII.I..II...I 364 I" " I'' " I" " I n/z~> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 ^bundance #52248: Heptacosane 57

38.00 38.20 38.40 38.60 5000 85 Wz 85.05 46.84%

TT-p-T

Tl/Z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 Abundance #74635: Hexatriacontane T ' ' ' 'I' 7 38.00 38.20 38.40 38.60 m/z 83705 30.66% 5000 85

■nZz-> " i''' j 1 11 I , 196 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 360 380 225 253 281 OwM 38.00 38.20 38.40 38.60

23322.D NP091101.M Mon Oct 15 10:26:23 2001 Page 17

NYC-WTC_000088286

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NYC-WTC_000088286Source: NYC Law Department, mirrored locally

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