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GC/MS analysis results for sample AD23322, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23322 conducted on October 15, 2001.

NYC-WTC_000088263–000088289

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088285
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1201\23322.D Vial: 15 Acq On : 12 Oct 2001 3:48 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 16 Heneicosane Concentration Rank 9

R.T. EstConc Area Relative to ISTD R.T. 36.36 1.60 ug/1 136305 Perylene-dl2 37.22 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Heneicosane 296 C21H44 000629-94-7 91 2 Tetratetracontane 619 C44H90 007098-22-8 91 3 Heptacosane 380 C27H56 000593-49-7 91 4 Hexatriacontane 507 C36H74 , 000630-06-8 9^ Abundance Scan 3412 (36.361 min): 23322.D (-) niTz 56.95 100.00% 5(7

5000 85

36.00 36.20 36.40 36.60 T—T— m/z 71.00 69.75% ■nfe-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #42201: Heneicosane 57

85 5000 .. 36.00 36.20 36.40 36.60 m/z 43.05 667^7% .................... ................................. ................................ •nZz-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #61068: Tetratetracontane 57

36.00 36.20 36.40 36.60 5000 m/z 85.05 48.00% 85 A

fPl41169197225 379407 590618 ' '1 ' ’ ' ' I ' ' ''''i ' ' ' '' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ‘ I ‘ ' I ' ' ' ' I ' ' Ti/z-> 50 100 150 200 250 300 350 400 450 500 550 600 Abundance #52248: Heptacosane ''i iCvn I 1 ,1 Ti I I /'i 57 36.00 36.20 36.40 36.60 tn/z 55.00 22.32%

5000 85

380 ''' I' '' ' I'''' I ''' ' I'' '' I '' I I ' ' ' ' I ' ' ■n/z-> 50 100 150 200 250 300 350 400 450 500 550 600 36.00 36.20 36.40 36.60

23322.D NP091101.M Mon Oct 15 10:26:21 2001 Page 16

NYC-WTC_000088285

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NYC-WTC_000088285Source: NYC Law Department, mirrored locally

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